2,3,6-trinitro-benzoic acid

Base Information

Chemical Name:2,3,6-trinitro-benzoic acid
CAS No.:102312-38-9
Molecular Formula:C₇H₃N₃O₈
Molecular Weight:257.116
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,6-trinitro-benzoic acid

Chemical Property:

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Technology Process of 2,3,6-trinitro-benzoic acid

There total 5 articles about 2,3,6-trinitro-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18292-97-2
2,3,6-trinitrotoluene

: 102312-38-9
2,3,6-trinitro-benzoic acid

Guidance literature:: With chromium(III) oxide; sulfuric acid; at 60 - 80 ℃;

Reference yield:

: 19406-51-0,153919-64-3
4-Amino-2,6-dinitrotoluene

: 102312-38-9
2,3,6-trinitro-benzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: sodium acetate; glacial acetic acid; bromine

2: absolute alcohol; ethyl nitrite / 380 Torr

3: alcohol; ammonia / 145 °C

4: nitric acid; N₂O₃ / 0 °C / Behandeln des entstandenen Diazoniumnitrats mit waessr. NaNO₂ und Erwaermen des Reaktionsprodukts mit konz. Salpetersaeure

5: Cr₂O₃-H₂SO₄ / 60 - 80 °C

With chromium(III) oxide; dinitrogen trioxide; ethyl nitrite; ethanol; sulfuric acid; ammonia; bromine; nitric acid; sodium acetate; acetic acid;

Reference yield:

: 10202-92-3
3-methyl-2,4-dinitroaniline

: 102312-38-9
2,3,6-trinitro-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: nitric acid; N₂O₃ / 0 °C / Behandeln des entstandenen Diazoniumnitrats mit waessr. NaNO₂ und Erwaermen des Reaktionsprodukts mit konz. Salpetersaeure

2: Cr₂O₃-H₂SO₄ / 60 - 80 °C

With chromium(III) oxide; dinitrogen trioxide; sulfuric acid; nitric acid;