Carbonic acid 6-[(7R,8R,9S,13S,14S,17S)-13-methyl-3,17-bis-(tetrahydro-pyran-2-yloxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl]-hexyl ester 4-nitro-phenyl ester

Base Information

• Chemical Name: Carbonic acid 6-[(7R,8R,9S,13S,14S,17S)-13-methyl-3,17-bis-(tetrahydro-pyran-2-yloxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl]-hexyl ester 4-nitro-phenyl ester
• CAS No.: 740809-80-7
• Molecular Formula: C₄₁H₅₅NO₉
• Molecular Weight: 705.889

Synonyms:

Chemical Property of Carbonic acid 6-[(7R,8R,9S,13S,14S,17S)-13-methyl-3,17-bis-(tetrahydro-pyran-2-yloxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl]-hexyl ester 4-nitro-phenyl ester

Chemical Property:

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Useful:

Technology Process of Carbonic acid 6-[(7R,8R,9S,13S,14S,17S)-13-methyl-3,17-bis-(tetrahydro-pyran-2-yloxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl]-hexyl ester 4-nitro-phenyl ester

There total 2 articles about Carbonic acid 6-[(7R,8R,9S,13S,14S,17S)-13-methyl-3,17-bis-(tetrahydro-pyran-2-yloxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl]-hexyl ester 4-nitro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-((7R,13S,14S,17S)-13-methyl-3,17-bis((tetrahydro-2H-pyran-2-yl)oxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl)hexan-1-ol (408512-83-4) → Carbonic acid 6-[(7R,8R,9S,13S,14S,17S)-13-methyl-3,17-bis-(tetrahydro-pyran-2-yloxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl]-hexyl ester 4-nitro-phenyl ester (740809-80-7)

Guidance literature:

Reference yield:

4-Nitrophenyl chloroformate (7693-46-1) + 6-((7R,13S,14S,17S)-13-methyl-3,17-bis((tetrahydro-2H-pyran-2-yl)oxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl)hexan-1-ol (408512-83-4) → Carbonic acid 6-[(7R,8R,9S,13S,14S,17S)-13-methyl-3,17-bis-(tetrahydro-pyran-2-yloxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl]-hexyl ester 4-nitro-phenyl ester (740809-80-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2004.04.064

Reference yield:

3-[4-[N,N-bis(2-chloroethyl)amino]-phenyl]-propylamine (129787-13-9) + Carbonic acid 6-[(7R,8R,9S,13S,14S,17S)-13-methyl-3,17-bis-(tetrahydro-pyran-2-yloxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl]-hexyl ester 4-nitro-phenyl ester (740809-80-7) → (3-{4-[Bis-(2-chloro-ethyl)-amino]-phenyl}-propyl)-carbamic acid 6-[(7R,8R,9S,13S,14S,17S)-13-methyl-3,17-bis-(tetrahydro-pyran-2-yloxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl]-hexyl ester

Guidance literature:

In tetrahydrofuran; water; Heating;

DOI:10.1016/j.bmcl.2004.04.064

upstream raw materials:

4-Nitrophenyl chloroformate

6-((7R,13S,14S,17S)-13-methyl-3,17-bis((tetrahydro-2H-pyran-2-yl)oxy)-7,8,9,11,12,13,14,15,16,17-decahydro-6H-cyclopenta[a]phenanthren-7-yl)hexan-1-ol

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