Technology Process of C24H29NO6
There total 7 articles about C24H29NO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
trimethylsulphonium iodide;
With
sodium hydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 0.916667h;
Inert atmosphere;
C23H27NO6;
In
tetrahydrofuran;
at 20 ℃;
for 6h;
Inert atmosphere;
DOI:10.1021/jo500493c
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sulfuric acid / methanol / 30 h / 20 °C / Inert atmosphere
2.1: (1S)-10-camphorsulfonic acid / toluene / 5 h / Reflux; Inert atmosphere
3.1: diisobutylaluminium hydride / dichloromethane / 0.25 h / -78 °C / Inert atmosphere
4.1: sodium hydride / tetrahydrofuran / 0.92 h / 0 - 20 °C / Inert atmosphere
4.2: 6 h / 20 °C / Inert atmosphere
With
sulfuric acid; (1S)-10-camphorsulfonic acid; sodium hydride; diisobutylaluminium hydride;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jo500493c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: (1S)-10-camphorsulfonic acid / toluene / 5 h / Reflux; Inert atmosphere
2.1: diisobutylaluminium hydride / dichloromethane / 0.25 h / -78 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran / 0.92 h / 0 - 20 °C / Inert atmosphere
3.2: 6 h / 20 °C / Inert atmosphere
With
(1S)-10-camphorsulfonic acid; sodium hydride; diisobutylaluminium hydride;
In
tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/jo500493c