(1S,4R)-1-<(1S)-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-<2-(4-chlorophenyl)-2-oxo-1-ethyl>-2-isoquinolylcarbonyl>-4,7,7-trimethyl-2-oxa-bicyclo<2.2.1>heptan-3-one

Base Information

Chemical Name:(1S,4R)-1-<(1S)-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-<2-(4-chlorophenyl)-2-oxo-1-ethyl>-2-isoquinolylcarbonyl>-4,7,7-trimethyl-2-oxa-bicyclo<2.2.1>heptan-3-one
CAS No.:123279-30-1
Molecular Formula:C₂₉H₃₂ClNO₆
Molecular Weight:526.029
Hs Code.:

(1S,4R)-1-<(1S)-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-<2-(4-chlorophenyl)-2-oxo-1-ethyl>-2-isoquinolylcarbonyl>-4,7,7-trimethyl-2-oxa-bicyclo<2.2.1>heptan-3-one

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Chemical Property of (1S,4R)-1-<(1S)-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-<2-(4-chlorophenyl)-2-oxo-1-ethyl>-2-isoquinolylcarbonyl>-4,7,7-trimethyl-2-oxa-bicyclo<2.2.1>heptan-3-one

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Technology Process of (1S,4R)-1-<(1S)-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-<2-(4-chlorophenyl)-2-oxo-1-ethyl>-2-isoquinolylcarbonyl>-4,7,7-trimethyl-2-oxa-bicyclo<2.2.1>heptan-3-one

There total 4 articles about (1S,4R)-1-<(1S)-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-<2-(4-chlorophenyl)-2-oxo-1-ethyl>-2-isoquinolylcarbonyl>-4,7,7-trimethyl-2-oxa-bicyclo<2.2.1>heptan-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39637-74-6
(1S)-(-)-camphanic chloride

: 123279-30-1
(1S,4R)-1-<(1S)-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-<2-(4-chlorophenyl)-2-oxo-1-ethyl>-2-isoquinolylcarbonyl>-4,7,7-trimethyl-2-oxa-bicyclo<2.2.1>heptan-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 90.4 percent / N(C₂H₅)3 / CH₂Cl₂ / 1) 0 deg C, 15 min, 2) RT, 4 h

2: triphenylcarbenium tetrafluoroborate / CH₂Cl₂ / 16 h / Ambient temperature

3: CH₂Cl₂ / 18 h / -78 °C / also with TiCl₄

With trityl tetrafluoroborate; triethylamine; In dichloromethane;
DOI:10.1002/ardp.19903230605

Reference yield:

: 123279-28-7
(1S,4R)-1-(6,7-Dimethoxy-1,2,3,4-tetrahydro-2-isoquinolylcarbonyl)-4,7,7-trimethyl-2-oxa-bicyclo<2.2.1>-heptan-3-one

: 123279-30-1
(1S,4R)-1-<(1S)-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-<2-(4-chlorophenyl)-2-oxo-1-ethyl>-2-isoquinolylcarbonyl>-4,7,7-trimethyl-2-oxa-bicyclo<2.2.1>heptan-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylcarbenium tetrafluoroborate / CH₂Cl₂ / 16 h / Ambient temperature

2: CH₂Cl₂ / 18 h / -78 °C / also with TiCl₄

With trityl tetrafluoroborate; In dichloromethane;
DOI:10.1002/ardp.19903230605

Reference yield:

: 2328-12-3
6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline monohydrochloride

: 123279-30-1
(1S,4R)-1-<(1S)-1,2,3,4-Tetrahydro-6,7-dimethoxy-1-<2-(4-chlorophenyl)-2-oxo-1-ethyl>-2-isoquinolylcarbonyl>-4,7,7-trimethyl-2-oxa-bicyclo<2.2.1>heptan-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 90.4 percent / N(C₂H₅)3 / CH₂Cl₂ / 1) 0 deg C, 15 min, 2) RT, 4 h

2: triphenylcarbenium tetrafluoroborate / CH₂Cl₂ / 16 h / Ambient temperature

3: CH₂Cl₂ / 18 h / -78 °C / also with TiCl₄

With trityl tetrafluoroborate; triethylamine; In dichloromethane;
DOI:10.1002/ardp.19903230605