Technology Process of C45H68O8S
There total 4 articles about C45H68O8S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
DL-thiomalic acid; C25H46O2;
With
dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
methanol;
Inert atmosphere;
4-Methoxybenzyl alcohol;
With
2,2-dimethylpropanoic anhydride;
In
tetrahydrofuran;
DOI:10.1007/s11746-014-2459-5
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / acetic acid / Inert atmosphere; Cooling with ice
2: eschenmoser's salt / 20 °C / Reflux
3: dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene / methanol / Inert atmosphere
With
dmap; sodium tetrahydroborate; eschenmoser's salt; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
methanol; acetic acid;
3: |Michael Addition;
DOI:10.1007/s11746-014-2459-5
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C
2: sodium tetrahydroborate / acetic acid / Inert atmosphere; Cooling with ice
3: eschenmoser's salt / 20 °C / Reflux
4: dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene / methanol / Inert atmosphere
With
dmap; sodium tetrahydroborate; eschenmoser's salt; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; dichloromethane; acetic acid;
4: |Michael Addition;
DOI:10.1007/s11746-014-2459-5
