1-carbonyl>amino>-2-cyclohexene

Base Information

• Chemical Name: 1-carbonyl>amino>-2-cyclohexene
• CAS No.: 132646-16-3
• Molecular Formula: C₁₉H₂₅NO₂
• Molecular Weight: 299.413

Synonyms:

Chemical Property of 1-carbonyl>amino>-2-cyclohexene

Chemical Property:

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Technology Process of 1-carbonyl>amino>-2-cyclohexene

There total 4 articles about 1-carbonyl>amino>-2-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H33NO3SSi → 1-carbonyl>amino>-2-cyclohexene (132646-16-3,132746-35-1)

Guidance literature:

With lithium hydroxide; water; In tetrahydrofuran; methanol; for 3h; Yield given; Ambient temperature;

DOI:10.1021/ja00009a045

Reference yield:

(S)-trans-2-phenylcyclohexyl carbamate (129966-10-5) → 1-carbonyl>amino>-2-cyclohexene (132646-16-3,132746-35-1)

Guidance literature:

Multi-step reaction with 4 steps

1: SOCl₂, pyridine / benzene / 14.25 h / Ambient temperature

2: SnCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

3: 1,2-dichloro-ethane / 1.) RT, 90 min, 2.) 50 deg C, 90 min, 3.) reflux, overnight

4: LiOH, H₂O / tetrahydrofuran; methanol / 3 h / Ambient temperature

With pyridine; lithium hydroxide; thionyl chloride; water; tin(IV) chloride; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane; benzene;

DOI:10.1021/ja00009a045

Reference yield:

(S)-trans-2-phenylcyclohexyl N-sulfinylcarbamate (107575-41-7,130060-02-5) → 1-carbonyl>amino>-2-cyclohexene (132646-16-3,132746-35-1)

Guidance literature:

Multi-step reaction with 3 steps

1: SnCl₄ / CH₂Cl₂ / 0.33 h / -78 °C

2: 1,2-dichloro-ethane / 1.) RT, 90 min, 2.) 50 deg C, 90 min, 3.) reflux, overnight

3: LiOH, H₂O / tetrahydrofuran; methanol / 3 h / Ambient temperature

With lithium hydroxide; water; tin(IV) chloride; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane;

DOI:10.1021/ja00009a045

upstream raw materials:

(S)-trans-2-phenylcyclohexyl carbamate

(S)-trans-2-phenylcyclohexyl N-sulfinylcarbamate

C₁₉H₂₅NO₃S

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