β-D-Glucopyranosyl 4-sec-Butyl-2-nitrophenyl Disulfide

Base Information

Chemical Name:β-D-Glucopyranosyl 4-sec-Butyl-2-nitrophenyl Disulfide
CAS No.:74752-45-7
Molecular Formula:C₁₆H₂₃NO₇S₂
Molecular Weight:405.493
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-D-Glucopyranosyl 4-sec-Butyl-2-nitrophenyl Disulfide

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Technology Process of β-D-Glucopyranosyl 4-sec-Butyl-2-nitrophenyl Disulfide

There total 5 articles about β-D-Glucopyranosyl 4-sec-Butyl-2-nitrophenyl Disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 10593-29-0
sodium 1-thio-β-D-glucopyranoside

: 74752-42-4
4-sec-Butyl-2-nitrobenzenesulfenyl Chloride

: 74752-45-7
β-D-Glucopyranosyl 4-sec-Butyl-2-nitrophenyl Disulfide

Guidance literature:: With 15-crown-5;
DOI:10.1021/jo01309a030

Reference yield:

: 3555-18-8
4-sec-butyl-2-nitrophenol

: 74752-45-7
β-D-Glucopyranosyl 4-sec-Butyl-2-nitrophenyl Disulfide

Guidance literature:: Multi-step reaction with 5 steps

1: NaH

2: Heating

3: 55 percent / K₂CO₃

4: 98 percent / SO₂Cl₂

5: 67 percent / 15-crown-5

With sulfuryl dichloride; 15-crown-5; sodium hydride; potassium carbonate;
DOI:10.1021/jo01309a030

Reference yield:

: 74752-39-9
4-sec-Butyl-2-nitrothiophenol

: 74752-45-7
β-D-Glucopyranosyl 4-sec-Butyl-2-nitrophenyl Disulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / SO₂Cl₂

2: 67 percent / 15-crown-5

With sulfuryl dichloride; 15-crown-5;
DOI:10.1021/jo01309a030