1-phenyl-2,5-bis(methylene)stibolane

Base Information

Chemical Name:1-phenyl-2,5-bis(methylene)stibolane
CAS No.:108035-98-9
Molecular Formula:C₁₂H₁₃Sb
Molecular Weight:278.985
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenyl-2,5-bis(methylene)stibolane

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Technology Process of 1-phenyl-2,5-bis(methylene)stibolane

There total 1 articles about 1-phenyl-2,5-bis(methylene)stibolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 5035-52-9
dichlorophenylstibine

: 108035-99-0
2,5-dilithio-1,5-hexadiene

: 108035-98-9
1-phenyl-2,5-bis(methylene)stibolane

Guidance literature:: In diethyl ether; ether soln. of CH2=CLi(CH2)2CLi=CH2 was added dropwise to a suspn. of PhSbCl2 at 25°C, stirred for 12 h; filtered, evapd., residue was extd. with pentane, ext. was evapd., residue was purified by Kugelrohr distn. (100°C at 0.005 Torr); elem. anal.;
DOI:10.1021/om00149a009