[PdCl(bis(2-picolyl)phenylphosphine-N,P,N)]PF₆

Base Information

Chemical Name:[PdCl(bis(2-picolyl)phenylphosphine-N,P,N)]PF₆
CAS No.:1223552-75-7
Molecular Formula:C₁₈H₁₇ClN₂PPd*F₆P
Molecular Weight:579.157
Hs Code.:

[PdCl(bis(2-picolyl)phenylphosphine-N,P,N)]PF<sub>6</sub>

Synonyms:

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Chemical Property of [PdCl(bis(2-picolyl)phenylphosphine-N,P,N)]PF₆

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Technology Process of [PdCl(bis(2-picolyl)phenylphosphine-N,P,N)]PF₆

There total 3 articles about [PdCl(bis(2-picolyl)phenylphosphine-N,P,N)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 60969-19-9
thallium(I) hexafluorophosphate

: 86674-25-1
phenylphosphino-bis(2-methylpyridine)

: 1223552-75-7
[PdCl(bis(2-picolyl)phenylphosphine-N,P,N)]PF₆

: [Pd2Cl2(μ-bis(2-picolyl)phenylphosphine)2](PF6)2

Guidance literature:: In tetrahydrofuran; byproducts: TlCl; (inert atm., Schlenk technique); addn. of palladium compd. to THF soln. of phosphine deriv., stirring overnight, addn. of thallium compd., stirring for 12 h; evapn., extn. (DMF), filtration, addn. of diethyl ether, filtration to give monopalladium compd. as ppt., washing with CH2Cl2, concg. combined filtrates, evapn. to give dipalladium compd., elem. anal.;
DOI:10.1039/b919679j

Reference yield:

: [Pd2Cl2(μ-bis(2-picolyl)phenylphosphine)2](PF6)2

: 1223552-75-7
[PdCl(bis(2-picolyl)phenylphosphine-N,P,N)]PF₆

Guidance literature:: In dimethyl sulfoxide; (inert atm., Schlenk technique); keeping soln. of palladium compd. in DMSO at room temp. for 4 d or for 10 h at 80°C;
DOI:10.1039/b919679j

Reference yield:

: 60969-19-9
thallium(I) hexafluorophosphate

: 1223552-73-5
[PdCl₂(bis(2-picolyl)phenylphosphine-N,P)]

: 1223552-75-7
[PdCl(bis(2-picolyl)phenylphosphine-N,P,N)]PF₆

Guidance literature:: In dimethylsulfoxide-d6; (inert atm., Schlenk technique); addn. of 1 equiv. of thallium compd. toDMSO-d6 soln. of palladium compd.;
DOI:10.1039/b919679j