N-(4-methoxyphenyl)-2-formylazetidine

Base Information

Chemical Name:N-(4-methoxyphenyl)-2-formylazetidine
CAS No.:1606993-66-1
Molecular Formula:C₁₁H₁₃NO₂
Molecular Weight:191.23
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-methoxyphenyl)-2-formylazetidine

Chemical Property:

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Technology Process of N-(4-methoxyphenyl)-2-formylazetidine

There total 2 articles about N-(4-methoxyphenyl)-2-formylazetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1606993-67-2
C₁₃H₁₇NO₃

: 1606993-66-1
N-(4-methoxyphenyl)-2-formylazetidine

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; toluene; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo500249c

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1606993-66-1
N-(4-methoxyphenyl)-2-formylazetidine

Guidance literature:: Multi-step reaction with 2 steps

1: N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydrogencarbonate / water; N,N-dimethyl-formamide / 4 h / 100 °C

2: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / -78 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; diisobutylaluminium hydride; sodium hydrogencarbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo500249c

Reference yield:

: 1606993-66-1
N-(4-methoxyphenyl)-2-formylazetidine

: 1606993-44-5
C₂₀H₂₁NO₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran; hexane / 20 h / 20 °C / Inert atmosphere

2.1: sulfuric acid / dichloromethane / 24 h / 0 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

3.2: 4 h / 20 °C / Inert atmosphere

With sulfuric acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane; dichloromethane; 2.1: |Aza-Claisen Rearrangement;
DOI:10.1021/jo500249c