N^α-Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteinyl-<2-(3-aminopyrrolidin-2-on-1yl)-4-methylpentanoyl>glycine Amide

Base Information

• Chemical Name: N^α-Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteinyl-<2-(3-aminopyrrolidin-2-on-1yl)-4-methylpentanoyl>glycine Amide
• CAS No.: 88463-36-9
• Molecular Formula: C₆₄H₈₄N₁₂O₁₄S₂
• Molecular Weight: 1309.57

Synonyms:

Chemical Property of N^α-Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteinyl-<2-(3-aminopyrrolidin-2-on-1yl)-4-methylpentanoyl>glycine Amide

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of N^α-Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteinyl-<2-(3-aminopyrrolidin-2-on-1yl)-4-methylpentanoyl>glycine Amide

There total 6 articles about N^α-Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteinyl-<2-(3-aminopyrrolidin-2-on-1yl)-4-methylpentanoyl>glycine Amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(3-Tert-butyloxycarbonylaminopyrrolidin-2-on-1-yl)-4-methylpentanoyl-glycine Amide (88463-34-7) → Nα-Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteinyl-<2-(3-aminopyrrolidin-2-on-1yl)-4-methylpentanoyl>glycine Amide (88463-36-9)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoracetic acid / 1 h / Ambient temperature

2: 83 mg / 1) N-hydroxybenzotriazol, 2) dicyclohexylcarbodiimide / dimethylformamide / 1) Room temp. 2) -lO deg C, 1 h, 3) room temp. 40 h

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In N,N-dimethyl-formamide;

DOI:10.1135/cccc19840642

Reference yield:

Methyl 2-(3-tert-butyloxycarbonylaminopyrrolidin-2-on-1-yl)-4-methylpentanoyl-glycinate (91682-44-9) → Nα-Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteinyl-<2-(3-aminopyrrolidin-2-on-1yl)-4-methylpentanoyl>glycine Amide (88463-36-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 0.52 g / Ammonia / methanol / 24 h

2: trifluoracetic acid / 1 h / Ambient temperature

3: 83 mg / 1) N-hydroxybenzotriazol, 2) dicyclohexylcarbodiimide / dimethylformamide / 1) Room temp. 2) -lO deg C, 1 h, 3) room temp. 40 h

With ammonia; benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In methanol; N,N-dimethyl-formamide;

DOI:10.1135/cccc19840642

Reference yield:

2-(3-Tert-butyloxycarbonylaminopyrrolidin-2-on-1-yl)-4-methylpentanoyl-glycine (88463-35-8) → Nα-Benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparaginyl-S-benzylcysteinyl-<2-(3-aminopyrrolidin-2-on-1yl)-4-methylpentanoyl>glycine Amide (88463-36-9)

Guidance literature:

Multi-step reaction with 4 steps

1: methanol; diethyl ether / 0.08 h

2: 0.52 g / Ammonia / methanol / 24 h

3: trifluoracetic acid / 1 h / Ambient temperature

4: 83 mg / 1) N-hydroxybenzotriazol, 2) dicyclohexylcarbodiimide / dimethylformamide / 1) Room temp. 2) -lO deg C, 1 h, 3) room temp. 40 h

With ammonia; benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In methanol; diethyl ether; N,N-dimethyl-formamide;

DOI:10.1135/cccc19840642

upstream raw materials:

2-(3-Aminopyrrolidin-2-on-1-yl)-4-methylpentanoyl-glycine Amide

N-benzyloxycarbonyl-S-benzylcysteinyl-tyrosyl-isoleucyl-glutaminyl-asparginyl-S-benzylcysteine

2-(3-Tert-butyloxycarbonylaminopyrrolidin-2-on-1-yl)-4-methylpentanoyl-glycine Amide

2-(3-Tert-butyloxycarbonylaminopyrrolidin-2-on-1-yl)-4-methylpentanoyl-glycine

Downstream raw materials:

<7,8-2-(3-Aminopyrrolidin-2-on-1-yl)-4-methylpentanoic acid>oxytocin

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