Technology Process of C17H20ClNO3
There total 6 articles about C17H20ClNO3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / acetone / Reflux
2: (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; dimethylsulfide borane complex / tetrahydrofuran / -10 °C
3: 1H-imidazole / N,N-dimethyl-formamide / 20 °C
4: sodium iodide / acetone / Reflux
5: triethylamine / N,N-dimethyl-formamide / 0 - 20 °C
6: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C
With
1H-imidazole; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; sodium iodide; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetone;
4: |Finkelstein Reaction;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium iodide / acetone / Reflux
2: triethylamine / N,N-dimethyl-formamide / 0 - 20 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C
With
tetrabutyl ammonium fluoride; triethylamine; sodium iodide;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetone;
1: |Finkelstein Reaction;