6',3-N,N-bis(tert-butyloxycarrbonyl)kanamycin A

Base Information

Chemical Name:6',3-N,N-bis(tert-butyloxycarrbonyl)kanamycin A
CAS No.:75178-77-7
Molecular Formula:C₂₈H₅₂N₄O₁₅
Molecular Weight:684.739
Hs Code.:

Synonyms:

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Chemical Property of 6',3-N,N-bis(tert-butyloxycarrbonyl)kanamycin A

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Technology Process of 6',3-N,N-bis(tert-butyloxycarrbonyl)kanamycin A

There total 1 articles about 6',3-N,N-bis(tert-butyloxycarrbonyl)kanamycin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 59-01-8
kanamycin A

: 75178-77-7
6',3-N,N-bis(tert-butyloxycarrbonyl)kanamycin A

Guidance literature:: With copper dichloride; Yield given. Multistep reaction; 1.) DMSO, RT, 24 h, 2.) DMSO, RT, 5 h;
DOI:10.1021/jm00023a011

Reference yield:

: 75178-77-7
6',3-N,N-bis(tert-butyloxycarrbonyl)kanamycin A

: 2-Amino-N-[(1R,2S,3S,4R,5S)-5-amino-2-((2S,3R,4S,5S,6R)-4-amino-3,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-4-((2R,3R,4S,5S,6R)-6-aminomethyl-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy)-3-hydroxy-cyclohexyl]-acetamide; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Cu(OAc)2*H₂O / 1.) DMF, RT, 4 h, 2.) DMF, RT, 24 h

2: 4 N HCl/THF / 2 h / Ambient temperature

With tetrahydrofuran; hydrogenchloride; copper diacetate;
DOI:10.1021/jm00023a011

Reference yield:

: 75178-77-7
6',3-N,N-bis(tert-butyloxycarrbonyl)kanamycin A

: C₂₄H₄₆N₆O₁₃*4ClH

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Cu(OAc)2*H₂O / 1.) DMF, RT, 4 h, 2.) DMF, RT, 24 h

2: 4 N HCl/THF / 2 h / Ambient temperature

With tetrahydrofuran; hydrogenchloride; copper diacetate;
DOI:10.1021/jm00023a011