Benzyl-[(S)-2-(dimethyl-phenyl-silanyl)-1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-ethyl]-amine

Base Information

Chemical Name:Benzyl-[(S)-2-(dimethyl-phenyl-silanyl)-1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-ethyl]-amine
CAS No.:161377-16-8
Molecular Formula:C₂₈H₃₉NO₅Si
Molecular Weight:497.707
Hs Code.:

Benzyl-[(S)-2-(dimethyl-phenyl-silanyl)-1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-ethyl]-amine

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Chemical Property of Benzyl-[(S)-2-(dimethyl-phenyl-silanyl)-1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-ethyl]-amine

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Technology Process of Benzyl-[(S)-2-(dimethyl-phenyl-silanyl)-1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-ethyl]-amine

There total 1 articles about Benzyl-[(S)-2-(dimethyl-phenyl-silanyl)-1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-ethyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107735-20-6
[(dimethylphenylsilyl)methyl]magnesium chloride

: Benzyl-[1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-meth-(E)-ylidene]-amine

: 161377-16-8
Benzyl-[(S)-2-(dimethyl-phenyl-silanyl)-1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-ethyl]-amine

Guidance literature:: With copper(l) iodide; boron trifluoride diethyl etherate; Yield given. Multistep reaction; 1.) - 40 deg C, 2.) -78 deg C;
DOI:10.1016/S0957-4166(00)86303-X

Reference yield:

: 161377-16-8
Benzyl-[(S)-2-(dimethyl-phenyl-silanyl)-1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-ethyl]-amine

: 76951-92-3
6-(benzyloxycarbonyl)amino-6-deoxy-1,2:3,4-di-O-isopropylidene-α-D-glycero-D-galacto-heptopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: NaHCO₃

2: 71 percent / KBr, CH₃COOOH

3: H₂ / Pd(OH)2

4: NaHCO₃

With peracetic acid; hydrogen; sodium hydrogencarbonate; potassium bromide; palladium dihydroxide;
DOI:10.1016/S0957-4166(00)86303-X

Reference yield:

: 161377-16-8
Benzyl-[(S)-2-(dimethyl-phenyl-silanyl)-1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-ethyl]-amine

: 161377-20-4
N-Benzyl-N-[(R)-2-hydroxy-1-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-yl)-ethyl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

2: KBr, CH₃COOOH

With peracetic acid; potassium bromide;
DOI:10.1016/S0957-4166(00)86303-X