Technology Process of C20H18N2O4S2
There total 3 articles about C20H18N2O4S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
tetrahydrofuran;
at 50 ℃;
for 18h;
DOI:10.1021/jm201546m
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Lawessons reagent / 1,4-dioxane / 2 h / 110 °C
2: ethanol / Reflux
3: potassium carbonate / tetrahydrofuran / 18 h / 50 °C
With
Lawessons reagent; potassium carbonate;
In
tetrahydrofuran; 1,4-dioxane; ethanol;
DOI:10.1021/jm201546m
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dihydrogen peroxide; potassium carbonate / water; dimethyl sulfoxide / 60 °C
2: Lawessons reagent / 1,4-dioxane / 2 h / 110 °C
3: ethanol / Reflux
4: potassium carbonate / tetrahydrofuran / 18 h / 50 °C
With
Lawessons reagent; dihydrogen peroxide; potassium carbonate;
In
tetrahydrofuran; 1,4-dioxane; ethanol; water; dimethyl sulfoxide;
DOI:10.1021/jm201546m