(S)-1-{3-[(R)-2-((S)-4-Amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethyldisulfanyl]-2-methyl-propionyl}-pyrrolidine-2-carboxylic acid

Base Information

• Chemical Name: (S)-1-{3-[(R)-2-((S)-4-Amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethyldisulfanyl]-2-methyl-propionyl}-pyrrolidine-2-carboxylic acid
• CAS No.: 103833-76-7
• Molecular Formula: C₁₉H₃₀N₄O₉S₂
• Molecular Weight: 522.601

Synonyms:

Chemical Property of (S)-1-{3-[(R)-2-((S)-4-Amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethyldisulfanyl]-2-methyl-propionyl}-pyrrolidine-2-carboxylic acid

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Technology Process of (S)-1-{3-[(R)-2-((S)-4-Amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethyldisulfanyl]-2-methyl-propionyl}-pyrrolidine-2-carboxylic acid

There total 2 articles about (S)-1-{3-[(R)-2-((S)-4-Amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethyldisulfanyl]-2-methyl-propionyl}-pyrrolidine-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3-mercapto-2-D-methyl-1-oxopropyl)-L-proline (78825-16-8) → (S)-1-(2-Methyl-3-methylsulfanyl-propionyl)-pyrrolidine-2-carboxylic acid (78636-29-0) + (S)-1-(3-Methanesulfinyl-2-methyl-propionyl)-pyrrolidine-2-carboxylic acid (78636-28-9) + C13(14)CH22N2O6S2 + D-2-methyl-3-mercaptopropionyl-l-prolin (62571-86-2,63250-36-2,64838-54-6,112243-88-6,112243-90-0,119238-52-7) + (S)-1-{3-[(R)-2-((S)-4-Amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethyldisulfanyl]-2-methyl-propionyl}-pyrrolidine-2-carboxylic acid (78636-30-3,103833-76-7)

Guidance literature:

urinary metabolites after oral administration to rats and dogs;

DOI:10.1248/cpb.29.1416

Reference yield:

glutathione disulfide (27025-41-8,40055-98-9,121-24-4,87140-29-2) + D-2-methyl-3-mercaptopropionyl-l-prolin (62571-86-2,63250-36-2,64838-54-6,112243-88-6,112243-90-0,119238-52-7) → glutathione (128960-77-0) + captopril disulfide (64838-57-9) + captopril-glutathione mixed disulfide (78636-30-3,103833-76-7)

Guidance literature:

With potassium chloride; edetate disodium; tert-butyl alcohol; In water-d2; Equilibrium constant;

DOI:10.1139/v85-006

upstream raw materials:

glutathione disulfide

D-2-methyl-3-mercaptopropionyl-l-prolin

1-(3-mercapto-2-D-methyl-1-oxopropyl)-L-proline

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