o-methoxy-N,O-dimethylhalostachine

Base Information

• Chemical Name: o-methoxy-N,O-dimethylhalostachine
• CAS No.: 125258-70-0
• Molecular Formula: C₁₂H₁₉NO₂
• Molecular Weight: 209.288
• Mol file: 125258-70-0.mol

Synonyms:

Chemical Property of o-methoxy-N,O-dimethylhalostachine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of o-methoxy-N,O-dimethylhalostachine

There total 3 articles about o-methoxy-N,O-dimethylhalostachine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Cr(CO)3(C6H4(OCH3)CHCH2N(CH3)2OCH3) → o-methoxy-N,O-dimethylhalostachine (125258-70-0)

Guidance literature:

decomplexation in air and sunlight; elem. anal.;

DOI:10.1016/0022-328X(89)87304-8

Reference yield:

(2-methoxyphenyl)methanol (612-16-8) → o-methoxy-N,O-dimethylhalostachine (125258-70-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) potassium hydride / 1.) THF, 21 h, 2.) THF, 1 h

With potassium hydride;

DOI:10.1016/S0957-4166(00)82088-1

Reference yield:

1-methoxy-2-methoxymethylbenzene (21998-86-7) + eschenmoser's salt (33797-51-2) → o-methoxy-N,O-dimethylhalostachine (125258-70-0)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1016/S0957-4166(00)82088-1

upstream raw materials:

1-methoxy-2-methoxymethylbenzene

eschenmoser's salt

(2-methoxyphenyl)methanol