(6S)-3,3-dimethyl-4ξ,8-dioxo-7c-(2-phenyl-acetylamino)-(6rH)-5-oxa-4λ⁴-thia-1-aza-bicyclo[4.2.0]octane-2t-carboxylic acid 4-nitro-benzyl ester

Base Information

• Chemical Name: (6S)-3,3-dimethyl-4ξ,8-dioxo-7c-(2-phenyl-acetylamino)-(6rH)-5-oxa-4λ⁴-thia-1-aza-bicyclo[4.2.0]octane-2t-carboxylic acid 4-nitro-benzyl ester
• CAS No.: 67807-68-5
• Molecular Formula: C₂₃H₂₃N₃O₈S
• Molecular Weight: 501.517

Synonyms:

Chemical Property of (6S)-3,3-dimethyl-4ξ,8-dioxo-7c-(2-phenyl-acetylamino)-(6rH)-5-oxa-4λ⁴-thia-1-aza-bicyclo[4.2.0]octane-2t-carboxylic acid 4-nitro-benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (6S)-3,3-dimethyl-4ξ,8-dioxo-7c-(2-phenyl-acetylamino)-(6rH)-5-oxa-4λ⁴-thia-1-aza-bicyclo[4.2.0]octane-2t-carboxylic acid 4-nitro-benzyl ester

There total 3 articles about (6S)-3,3-dimethyl-4ξ,8-dioxo-7c-(2-phenyl-acetylamino)-(6rH)-5-oxa-4λ⁴-thia-1-aza-bicyclo[4.2.0]octane-2t-carboxylic acid 4-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid 4-nitro-benzyl ester (67807-58-3) → (6S)-3,3-dimethyl-4ξ,8-dioxo-7c-(2-phenyl-acetylamino)-(6rH)-5-oxa-4λ4-thia-1-aza-bicyclo[4.2.0]octane-2t-carboxylic acid 4-nitro-benzyl ester (67807-68-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

Reference yield:

(4-nitrophenyl)diazomethane (19479-80-2) → (6S)-3,3-dimethyl-4ξ,8-dioxo-7c-(2-phenyl-acetylamino)-(6rH)-5-oxa-4λ4-thia-1-aza-bicyclo[4.2.0]octane-2t-carboxylic acid 4-nitro-benzyl ester (67807-68-5)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) H₂S, CH₂Cl₂, (ii) /BRN= 512396/, Et₂O

2: MCPBA / CH₂Cl₂

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

Reference yield:

(S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid; mercury(II) salt (1:1) (52512-70-6) → (6S)-3,3-dimethyl-4ξ,8-dioxo-7c-(2-phenyl-acetylamino)-(6rH)-5-oxa-4λ4-thia-1-aza-bicyclo[4.2.0]octane-2t-carboxylic acid 4-nitro-benzyl ester (67807-68-5)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) H₂S, CH₂Cl₂, (ii) /BRN= 512396/, Et₂O

2: MCPBA / CH₂Cl₂

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

upstream raw materials:

(S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid 4-nitro-benzyl ester

(4-nitrophenyl)diazomethane

(S)-2-((1S)-3-benzyl-7-oxo-(1rH,5cH)-4-oxa-2,6-diaza-bicyclo[3.2.0]hept-2-en-6-yl)-3-mercapto-3-methyl-butyric acid; mercury(II) salt (1:1)

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