S-2-benzoylbutyl acetothiolate

Base Information

• Chemical Name: S-2-benzoylbutyl acetothiolate
• CAS No.: 196702-56-4
• Molecular Formula: C₁₃H₁₆O₂S
• Molecular Weight: 236.335

Synonyms:

Chemical Property of S-2-benzoylbutyl acetothiolate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of S-2-benzoylbutyl acetothiolate

There total 1 articles about S-2-benzoylbutyl acetothiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

4-((Z)-1-Phenyl-but-1-enyl)-morpholine + N,N-bis(acetylthiomethyl)-p-chloroaniline (127099-06-3) → S-2-benzoylbutyl acetothiolate (196702-56-4)

Guidance literature:

With trifluoroacetic acid; In acetonitrile; for 1h; Heating;

DOI:10.1016/S0957-4166(97)00281-4

Reference yield: 43.0%

S-2-benzoylbutyl acetothiolate (196702-56-4) → (R)-2-Mercaptomethyl-1-phenyl-butan-1-one

Guidance literature:

With lipase AH; water; In di-isopropyl ether; for 32h; Ambient temperature;

DOI:10.1016/S0957-4166(97)00281-4

Reference yield:

S-2-benzoylbutyl acetothiolate (196702-56-4) → (S)-2-methyl-1-phenylbutan-1-one (16725-76-1)

Guidance literature:

Multi-step reaction with 2 steps

2: Raney Ni

With nickel;

DOI:10.1016/S0957-4166(97)00281-4

upstream raw materials:

N,N-bis(acetylthiomethyl)-p-chloroaniline

Downstream raw materials:

(S)-2-methyl-1-phenylbutan-1-one

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