C₁₅H₂₅NO

Base Information

Chemical Name:C₁₅H₂₅NO
CAS No.:1359985-32-2
Molecular Formula:C₁₅H₂₅NO
Molecular Weight:235.37
Hs Code.:

Synonyms:

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Chemical Property of C₁₅H₂₅NO

Chemical Property:

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Technology Process of C₁₅H₂₅NO

There total 13 articles about C₁₅H₂₅NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₁₆O₄

: 1359985-32-2
C₁₅H₂₅NO

Guidance literature:: Multi-step reaction with 11 steps

1: diphenyl phosphoryl azide; triethylamine / toluene / 1 h / 70 °C

2: triethylamine / toluene / 5 h / 80 °C

3: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 5 h / 20 °C

4: borane-THF / tetrahydrofuran / 4 h / -5 °C

5: Chiral Pak AD-H 250 column / ethanol; carbon dioxide / 40 °C / Resolution of racemate

6: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 2585.81 Torr

7: acetic acid / toluene / 2 h / Reflux

8: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

9: diethyl ether / 0.5 h / 0 °C

10: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

11: diethyl ether / 0.5 h / 0 °C

With tetrapropylammonium perruthennate; borane-THF; lithium hydroxide monohydrate; diphenyl phosphoryl azide; palladium 10% on activated carbon; water; hydrogen; acetic acid; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; carbon dioxide; toluene; 2: Curtius rearrangement / 9: Grignard reaction / 11: Grignard reaction;
DOI:10.1055/s-0031-1289884

Reference yield:

: C₁₇H₂₃NO₄

: 1359985-32-2
C₁₅H₂₅NO

Guidance literature:: Multi-step reaction with 9 steps

1: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 5 h / 20 °C

2: borane-THF / tetrahydrofuran / 4 h / -5 °C

3: Chiral Pak AD-H 250 column / ethanol; carbon dioxide / 40 °C / Resolution of racemate

4: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 2585.81 Torr

5: acetic acid / toluene / 2 h / Reflux

6: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

7: diethyl ether / 0.5 h / 0 °C

8: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

9: diethyl ether / 0.5 h / 0 °C

With tetrapropylammonium perruthennate; borane-THF; lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; acetic acid; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; carbon dioxide; toluene; 7: Grignard reaction / 9: Grignard reaction;
DOI:10.1055/s-0031-1289884

Reference yield:

: C₁₀H₁₅N₃O₃

: 1359985-32-2
C₁₅H₂₅NO

Guidance literature:: Multi-step reaction with 10 steps

1: triethylamine / toluene / 5 h / 80 °C

2: lithium hydroxide monohydrate; water / tetrahydrofuran; methanol / 5 h / 20 °C

3: borane-THF / tetrahydrofuran / 4 h / -5 °C

4: Chiral Pak AD-H 250 column / ethanol; carbon dioxide / 40 °C / Resolution of racemate

5: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 2585.81 Torr

6: acetic acid / toluene / 2 h / Reflux

7: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

8: diethyl ether / 0.5 h / 0 °C

9: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 2 h / Molecular sieve

10: diethyl ether / 0.5 h / 0 °C

With tetrapropylammonium perruthennate; borane-THF; lithium hydroxide monohydrate; palladium 10% on activated carbon; water; hydrogen; acetic acid; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; carbon dioxide; toluene; 1: Curtius rearrangement / 8: Grignard reaction / 10: Grignard reaction;
DOI:10.1055/s-0031-1289884