C₂₉H₃₁ClF₃N₃O₂S

Base Information

• Chemical Name: C₂₉H₃₁ClF₃N₃O₂S
• CAS No.: 1392267-26-3
• Molecular Formula: C₂₉H₃₁ClF₃N₃O₂S
• Molecular Weight: 578.098
• Mol file: 1392267-26-3.mol

Synonyms:

Chemical Property of C₂₉H₃₁ClF₃N₃O₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₃₁ClF₃N₃O₂S

There total 6 articles about C₂₉H₃₁ClF₃N₃O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

S-ethyl 3,3,4,4,4-pentafluoro-2-(2-oxo-2-phenylethyl)butanethioate (698348-08-2) → C29H31ClF3N3O2S (1392267-26-3)

Guidance literature:

Multi-step reaction with 2 steps

1: diisopropylamine / diethyl ether / 15 h / 20 °C

2: methanol / 20 °C

With diisopropylamine; In methanol; diethyl ether;

DOI:10.1021/jm301076q

Reference yield:

Bis(ethylthio)(heptafluoropropyl)methane (145327-73-7) → C29H31ClF3N3O2S (1392267-26-3)

Guidance literature:

Multi-step reaction with 5 steps

1: potassium hydroxide; tetrabutylammomium bromide / dichloromethane; water

2: potassium hydride / tetrahydrofuran / 0 °C

3: water; trifluoroacetic acid / Reflux

4: diisopropylamine / diethyl ether / 15 h / 20 °C

5: methanol / 20 °C

With tetrabutylammomium bromide; water; potassium hydride; diisopropylamine; trifluoroacetic acid; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;

DOI:10.1021/jm301076q

Reference yield:

Bis(ethylthio)(1,2,2,3,3,3-hexafluoropropylidene)methane (145327-77-1) → C29H31ClF3N3O2S (1392267-26-3)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium hydride / tetrahydrofuran / 0 °C

2: water; trifluoroacetic acid / Reflux

3: diisopropylamine / diethyl ether / 15 h / 20 °C

4: methanol / 20 °C

With water; potassium hydride; diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; diethyl ether;

DOI:10.1021/jm301076q

upstream raw materials:

4,7-dichloroquinoline

N-(6-aminohexyl)-7-chloroquinolin-4-amine

S-ethyl 3,3,4,4,4-pentafluoro-2-(2-oxo-2-phenylethyl)butanethioate

Bis(ethylthio)(heptafluoropropyl)methane