C₅₄H₆₀O₁₂

Base Information

Chemical Name:C₅₄H₆₀O₁₂
CAS No.:131147-17-6
Molecular Formula:C₅₄H₆₀O₁₂
Molecular Weight:901.063
Hs Code.:

C<sub>54</sub>H<sub>60</sub>O<sub>12</sub>

Synonyms:

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Chemical Property of C₅₄H₆₀O₁₂

Chemical Property:

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Technology Process of C₅₄H₆₀O₁₂

There total 36 articles about C₅₄H₆₀O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 131147-17-6,131233-77-7
C₅₄H₆₀O₁₂

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / dimethylformamide

2: M HCl / methanol / 0.5 h / Heating

3: 1) tetrabutylammonium bromide, dibutyltin oxide / 1) toluene, 2 h, reflux, 2) 2 h, reflux

4: toluene-p-sulphonic acid monohydrate / 10percent Pd-C / ethanol; H₂O / 11 h / Heating

5: 1) dibutyltin oxide, tetrabutylammonium bromide / 1) toluene, 2 h, reflux, 2) 7 h, reflux

6: pyridine / 12 h / 20 °C

With pyridine; hydrogenchloride; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)80132-M

Reference yield:

: 100-39-0
benzyl bromide

: 131147-17-6,131233-77-7
C₅₄H₆₀O₁₂

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydride / dimethylformamide

2: M HCl / methanol / 0.5 h / Heating

3: 1) tetrabutylammonium bromide, dibutyltin oxide / 1) toluene, 2 h, reflux, 2) 2 h, reflux

4: toluene-p-sulphonic acid monohydrate / 10percent Pd-C / ethanol; H₂O / 11 h / Heating

5: 1) dibutyltin oxide, tetrabutylammonium bromide / 1) toluene, 2 h, reflux, 2) 7 h, reflux

6: 54 mg / pyridine / 12 h / 20 °C

With pyridine; hydrogenchloride; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)80132-M

Reference yield:

: 58706-24-4,58769-25-8,98974-91-5,111466-16-1
(±)-3-O-benzyl-1,2:4,5-di-O-isopropylidene-myo-inositol

: 131147-17-6,131233-77-7
C₅₄H₆₀O₁₂

Guidance literature:: Multi-step reaction with 8 steps

1: sodium hydride / dimethylformamide

2: 49 percent / toluene-p-sulphonic acid monohydrate / acetone; H₂O / 0.75 h / 25 °C

3: sodium hydride / dimethylformamide

4: M HCl / methanol / 0.75 h / Heating

5: potassium tert-butoxide / dimethylsulfoxide / 2 h / 50 °C

6: 78 percent / M HCl / methanol / 0.5 h / Heating

7: 1) dibutyltin oxide, tetrabutylammonium bromide / 1) toluene, 2 h, reflux, 2) 7 h, reflux

8: pyridine / 12 h / 20 °C

With pyridine; hydrogenchloride; potassium tert-butylate; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; toluene-4-sulfonic acid; In methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone;
DOI:10.1016/0008-6215(90)80132-M