C₂₃H₂₃NO₄S

Base Information

Chemical Name:C₂₃H₂₃NO₄S
CAS No.:1354817-72-3
Molecular Formula:C₂₃H₂₃NO₄S
Molecular Weight:409.506
Hs Code.:

C<sub>23</sub>H<sub>23</sub>NO<sub>4</sub>S

Synonyms:

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Chemical Property of C₂₃H₂₃NO₄S

Chemical Property:

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Technology Process of C₂₃H₂₃NO₄S

There total 8 articles about C₂₃H₂₃NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 1354817-72-3
C₂₃H₂₃NO₄S

Guidance literature:: Multi-step reaction with 8 steps

1: morpholine / Reflux

2: 2-methyltetrahydrofuran / 20 °C

3: acetic acid; sulfuric acid / 15 h / 110 °C

4: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / N,N-dimethyl-formamide

5: n-butyllithium / tetrahydrofuran / -78 °C

6: hydrogenchloride; water / 1,4-dioxane / 1.5 h / 100 °C

7: potassium carbonate / N,N-dimethyl acetamide

8: L-proline; copper(l) iodide; sodium hydroxide / dimethyl sulfoxide

With morpholine; hydrogenchloride; copper(l) iodide; n-butyllithium; sulfuric acid; water; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; L-proline; sodium hydroxide; In tetrahydrofuran; 2-methyltetrahydrofuran; 1,4-dioxane; N,N-dimethyl acetamide; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.017

Reference yield:

: 42205-33-4,18861-58-0
ethyl 3-(4-bromophenyl)-2-cyanoacrylate

: 1354817-72-3
C₂₃H₂₃NO₄S

Guidance literature:: Multi-step reaction with 7 steps

1: 2-methyltetrahydrofuran / 20 °C

2: acetic acid; sulfuric acid / 15 h / 110 °C

3: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / N,N-dimethyl-formamide

4: n-butyllithium / tetrahydrofuran / -78 °C

5: hydrogenchloride; water / 1,4-dioxane / 1.5 h / 100 °C

6: potassium carbonate / N,N-dimethyl acetamide

7: L-proline; copper(l) iodide; sodium hydroxide / dimethyl sulfoxide

With hydrogenchloride; copper(l) iodide; n-butyllithium; sulfuric acid; water; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; L-proline; sodium hydroxide; In tetrahydrofuran; 2-methyltetrahydrofuran; 1,4-dioxane; N,N-dimethyl acetamide; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.017

Reference yield:

: 1354808-43-7
3-(4-bromophenyl)-3-o-tolylpropanoic acid

: 1354817-72-3
C₂₃H₂₃NO₄S

Guidance literature:: Multi-step reaction with 5 steps

1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine / N,N-dimethyl-formamide

2: n-butyllithium / tetrahydrofuran / -78 °C

3: hydrogenchloride; water / 1,4-dioxane / 1.5 h / 100 °C

4: potassium carbonate / N,N-dimethyl acetamide

5: L-proline; copper(l) iodide; sodium hydroxide / dimethyl sulfoxide

With hydrogenchloride; copper(l) iodide; n-butyllithium; water; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; L-proline; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl acetamide; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.017