Benzoic acid 2-benzenesulfonyl-4-((4R,5R)-5-dec-9-enyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-[2-((4R,5R)-5-decyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-butyl ester

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Chemical Name:Benzoic acid 2-benzenesulfonyl-4-((4R,5R)-5-dec-9-enyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-[2-((4R,5R)-5-decyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-butyl ester
CAS No.:202067-15-0
Molecular Formula:C₄₉H₇₆O₈S
Molecular Weight:825.204
Hs Code.:

Benzoic acid 2-benzenesulfonyl-4-((4R,5R)-5-dec-9-enyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-[2-((4R,5R)-5-decyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-butyl ester

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Chemical Property of Benzoic acid 2-benzenesulfonyl-4-((4R,5R)-5-dec-9-enyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-[2-((4R,5R)-5-decyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-butyl ester

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Technology Process of Benzoic acid 2-benzenesulfonyl-4-((4R,5R)-5-dec-9-enyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-[2-((4R,5R)-5-decyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-butyl ester

There total 6 articles about Benzoic acid 2-benzenesulfonyl-4-((4R,5R)-5-dec-9-enyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-[2-((4R,5R)-5-decyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 98-88-4
benzoyl chloride

: 202067-14-9
3-((4R,5R)-5-Decyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-propionaldehyde

: 202067-13-8
(4R,5R)-4-(3-Benzenesulfonyl-propyl)-5-dec-9-enyl-2,2-dimethyl-[1,3]dioxolane

: 202067-15-0
Benzoic acid 2-benzenesulfonyl-4-((4R,5R)-5-dec-9-enyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-[2-((4R,5R)-5-decyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-butyl ester

Guidance literature:: With n-butyllithium; In tetrahydrofuran; 1.) -78 deg C, 30 min, 2.) -78 deg C to r.t.;
DOI:10.1002/anie.199726321

Reference yield:

: 59101-26-7
pentadeca-4t,14-dien-1-ol

: 202067-15-0
Benzoic acid 2-benzenesulfonyl-4-((4R,5R)-5-dec-9-enyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-[2-((4R,5R)-5-decyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / aq. K₃Fe(CN)6, CH₃SO₂NH₂, OsO₄, (DHQD)2PHAL / 2-methyl-propan-2-ol

2: 94 percent / TsOH / benzene / 60 °C

3: 98 percent / H₂ / Pd/C / ethanol / 760 Torr / Ambient temperature

4: 98 percent / Dess-Martin periodinane / CH₂Cl₂ / Ambient temperature

5: 74 percent / BuLi / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) -78 deg C to r.t.

With osmium(VIII) oxide; n-butyllithium; methanesulfonamide; hydrogen; Dess-Martin periodane; toluene-4-sulfonic acid; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; tert-butyl alcohol; benzene;
DOI:10.1002/anie.199726321

Reference yield:

: Pentadec-14-ene-1,4,5-triol

: 202067-15-0
Benzoic acid 2-benzenesulfonyl-4-((4R,5R)-5-dec-9-enyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-[2-((4R,5R)-5-decyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-ethyl]-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / TsOH / benzene / 60 °C

2: 98 percent / H₂ / Pd/C / ethanol / 760 Torr / Ambient temperature

3: 98 percent / Dess-Martin periodinane / CH₂Cl₂ / Ambient temperature

4: 74 percent / BuLi / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) -78 deg C to r.t.

With n-butyllithium; hydrogen; Dess-Martin periodane; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; benzene;
DOI:10.1002/anie.199726321