Imidazole-1-carbothioic acid O-{(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[2-(dimethylamino-methyleneamino)-6-oxo-1,6-dihydro-purin-9-yl]-4-triisopropylsilanyloxy-tetrahydro-furan-3-yl} ester

Base Information

Chemical Name:Imidazole-1-carbothioic acid O-{(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[2-(dimethylamino-methyleneamino)-6-oxo-1,6-dihydro-purin-9-yl]-4-triisopropylsilanyloxy-tetrahydro-furan-3-yl} ester
CAS No.:1053251-34-5
Molecular Formula:C₄₇H₅₈N₈O₇SSi
Molecular Weight:907.178
Hs Code.:

Imidazole-1-carbothioic acid O-{(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[2-(dimethylamino-methyleneamino)-6-oxo-1,6-dihydro-purin-9-yl]-4-triisopropylsilanyloxy-tetrahydro-furan-3-yl} ester

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Chemical Property of Imidazole-1-carbothioic acid O-{(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[2-(dimethylamino-methyleneamino)-6-oxo-1,6-dihydro-purin-9-yl]-4-triisopropylsilanyloxy-tetrahydro-furan-3-yl} ester

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Imidazole-1-carbothioic acid O-{(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[2-(dimethylamino-methyleneamino)-6-oxo-1,6-dihydro-purin-9-yl]-4-triisopropylsilanyloxy-tetrahydro-furan-3-yl} ester

There total 6 articles about Imidazole-1-carbothioic acid O-{(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[2-(dimethylamino-methyleneamino)-6-oxo-1,6-dihydro-purin-9-yl]-4-triisopropylsilanyloxy-tetrahydro-furan-3-yl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 1053251-34-5
Imidazole-1-carbothioic acid O-{(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[2-(dimethylamino-methyleneamino)-6-oxo-1,6-dihydro-purin-9-yl]-4-triisopropylsilanyloxy-tetrahydro-furan-3-yl} ester

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / imidazole / dimethylformamide / 27 h / 25 °C

2: dimethylformamide / 100 h / 24 °C

With 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1021/jo00103a014

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 1053251-34-5
Imidazole-1-carbothioic acid O-{(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[2-(dimethylamino-methyleneamino)-6-oxo-1,6-dihydro-purin-9-yl]-4-triisopropylsilanyloxy-tetrahydro-furan-3-yl} ester

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / pyridine / 26 h / 25 °C

2: 50 percent / imidazole / dimethylformamide / 27 h / 25 °C

3: dimethylformamide / 100 h / 24 °C

With pyridine; 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1021/jo00103a014

Reference yield:

: 118-00-3
G

: 1053251-34-5
Imidazole-1-carbothioic acid O-{(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-[2-(dimethylamino-methyleneamino)-6-oxo-1,6-dihydro-purin-9-yl]-4-triisopropylsilanyloxy-tetrahydro-furan-3-yl} ester

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / methanol / 96 h / 27 °C

2: 96 percent / pyridine / 26 h / 25 °C

3: 50 percent / imidazole / dimethylformamide / 27 h / 25 °C

4: dimethylformamide / 100 h / 24 °C

With pyridine; 1H-imidazole; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jo00103a014