(1α,6α)-7-bicyclo<4.2.0>octan-7-ol

Base Information

• Chemical Name: (1α,6α)-7-bicyclo<4.2.0>octan-7-ol
• CAS No.: 131186-61-3
• Molecular Formula: C₁₆H₂₂O₄S
• Molecular Weight: 310.414

Synonyms:

Chemical Property of (1α,6α)-7-bicyclo<4.2.0>octan-7-ol

Chemical Property:

Purity/Quality:

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Technology Process of (1α,6α)-7-bicyclo<4.2.0>octan-7-ol

There total 2 articles about (1α,6α)-7-bicyclo<4.2.0>octan-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(1α,6α)-7-Acetoxy-7-bicyclo<4.2.0>octane (131186-60-2,131235-38-6) → (1α,6α)-7-bicyclo<4.2.0>octan-7-ol (131186-61-3,131235-39-7)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at -10 ℃; for 0.75h;

DOI:10.1016/S0040-4020(01)85603-9

Reference yield:

phenyl methoxymethyl sulfone (15251-78-2) + cis-bicyclo-[4.2.0]-octan-7-one (27655-70-5) → (1α,6α)-7-bicyclo<4.2.0>octan-7-ol (131186-61-3,131235-39-7)

Guidance literature:

With tert.-butyl lithium; Multistep reaction; 1) DME, -78 deg C, 2) -78 deg C;

DOI:10.1016/S0040-4020(01)85603-9

Reference yield:

acetic anhydride (108-24-7) + (1α,6α)-7-bicyclo<4.2.0>octan-7-ol (131186-61-3,131235-39-7) → (1α,6α)-7-Acetoxy-7-bicyclo<4.2.0>octane (131186-60-2,131235-38-6)

Guidance literature:

With dmap; In dichloromethane; Yield given; Ambient temperature;

DOI:10.1016/S0040-4020(01)85603-9

upstream raw materials:

phenyl methoxymethyl sulfone

cis-bicyclo-[4.2.0]-octan-7-one

(1α,6α)-7-Acetoxy-7-bicyclo<4.2.0>octane

Downstream raw materials:

(1α,6α)-7-Acetoxy-7-bicyclo<4.2.0>octane

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