(2RS,3RS,4SR,6SR)-3,4-epoxy-2,4-dimethyl-6-phenyl-tetrahydropyran

Base Information

Chemical Name:(2RS,3RS,4SR,6SR)-3,4-epoxy-2,4-dimethyl-6-phenyl-tetrahydropyran
CAS No.:98203-03-3
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

Synonyms:

Suppliers and Price of (2RS,3RS,4SR,6SR)-3,4-epoxy-2,4-dimethyl-6-phenyl-tetrahydropyran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2RS,3RS,4SR,6SR)-3,4-epoxy-2,4-dimethyl-6-phenyl-tetrahydropyran

Chemical Property:

Purity/Quality:

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Technology Process of (2RS,3RS,4SR,6SR)-3,4-epoxy-2,4-dimethyl-6-phenyl-tetrahydropyran

There total 32 articles about (2RS,3RS,4SR,6SR)-3,4-epoxy-2,4-dimethyl-6-phenyl-tetrahydropyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 98203-03-3,98301-07-6,98301-08-7,98301-09-8
(2RS,3SR,4RS,6SR)-3,4-epoxy-2,4-dimethyl-6-phenyl-tetrahydropyran

Guidance literature:: Multi-step reaction with 5 steps

1: 2.) KHSO₄ / 1.) H₂SO₄ / 1.) 2 d, room temp.; 2.) 140 degC, 27 mbar

2: m-chloroperbenzoic acid / CH₂Cl₂ / 2 h / Ambient temperature

3: 18.5 mg / LiAlH₄ / diethyl ether / 2 h / Heating

4: 21.5 percent / 20percent H₂SO₄ / H₂O / 6 h / 120 °C

5: m-chloroperbenzoic acid / CH₂Cl₂ / 2 h / Ambient temperature

With potassium hydrogensulfate; lithium aluminium tetrahydride; sulfuric acid; 3-chloro-benzenecarboperoxoic acid; sulfuric acid; In diethyl ether; dichloromethane; water;
DOI:10.1016/S0040-4020(01)96414-2

Reference yield:

: 100-52-7
benzaldehyde

: 98203-03-3,98301-07-6,98301-08-7,98301-09-8
(2RS,3SR,4RS,6RS)-3,4-epoxy-2,4-dimethyl-6-phenyl-tetrahydropyran

Guidance literature:: Multi-step reaction with 5 steps

1: 2.) KHSO₄ / 1.) H₂SO₄ / 1.) 2 d, room temp.; 2.) 140 degC, 27 mbar

2: m-chloroperbenzoic acid / CH₂Cl₂ / 2 h / Ambient temperature

3: 18.5 mg / LiAlH₄ / diethyl ether / 2 h / Heating

4: 64 percent / 20percent H₂SO₄ / H₂O / 6 h / 120 °C

5: m-chloperbenzoic acid / CH₂Cl₂ / 2 h / Ambient temperature

With potassium hydrogensulfate; lithium aluminium tetrahydride; sulfuric acid; 3-chloro-benzenecarboperoxoic acid; sulfuric acid; In diethyl ether; dichloromethane; water;
DOI:10.1016/S0040-4020(01)96414-2

Reference yield:

: 100-52-7
benzaldehyde

: 98203-03-3,98301-07-6,98301-08-7,98301-09-8
(2RS,3RS,4SR,6RS)-3,4-epoxy-2,4-dimethyl-6-phenyl-tetrahydropyran

Guidance literature:: Multi-step reaction with 5 steps

1: 2.) KHSO₄ / 1.) H₂SO₄ / 1.) 2 d, room temp.; 2.) 140 degC, 27 mbar

2: m-chloroperbenzoic acid / CH₂Cl₂ / 2 h / Ambient temperature

3: 18.5 mg / LiAlH₄ / diethyl ether / 2 h / Heating

4: 64 percent / 20percent H₂SO₄ / H₂O / 6 h / 120 °C

5: m-chloperbenzoic acid / CH₂Cl₂ / 2 h / Ambient temperature

With potassium hydrogensulfate; lithium aluminium tetrahydride; sulfuric acid; 3-chloro-benzenecarboperoxoic acid; sulfuric acid; In diethyl ether; dichloromethane; water;
DOI:10.1016/S0040-4020(01)96414-2