Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃

Base Information

• Chemical Name: Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃
• CAS No.: 98736-62-0
• Molecular Formula: CF₃O₃S*C₂₈H₂₂CrN₂O₂
• Molecular Weight: 619.561

Synonyms:

Chemical Property of Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃

Chemical Property:

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Useful:

Technology Process of Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃

There total 1 articles about Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chromium(II)trifluoromethanesulfonate + N,N'-ethylenebis(α-phenylsalicylideneiminate) (65940-45-6) → Cr(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O)(1+)*CF3SO2O(1-)=(Cr(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O))OSO2CF3 (98736-62-0)

Guidance literature:

With air; In acetone; Cr(OTf)2 in acetone was added dropwise under Ar to a suspn. of Ph2salenH2 in acetone, mixt. was stirred for 30 min, exposed to air and stirred for an addnl. hour; water was added, mixt. was stirred for 15 min, concd. in vacuo, filtered, ppt. was washed with deionized water and dried in air;

DOI:10.1021/ja00311a064

Reference yield:

Cr(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O)(1+)*CF3SO2O(1-)=(Cr(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O))OSO2CF3 (98736-62-0) + iodosylbenzene (536-80-1) → Cr(O)(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O)(1+)*CF3SO2O(1-)=(Cr(O)(OC6H4C(C6H5)NCH2CH2NC(C6H5)C6H4O))OSO2CF3 (98736-79-9)

Guidance literature:

In acetonitrile; a suspn. of Cr-complex and PhIO in MeCN was stirred for 30 min; soln. was filtered, anhyd. ether added to the filtrate, resulting ppt. was collected by filtration;

DOI:10.1021/ja00311a064

upstream raw materials:

N,N'-ethylenebis(α-phenylsalicylideneiminate)

Downstream raw materials:

Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O)⁽¹⁺⁾*CF₃SO₂O^(1-)=(Cr(O)(OC₆H₄C(C₆H₅)NCH₂CH₂NC(C₆H₅)C₆H₄O))OSO₂CF₃

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