(3S,7aR)-6-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetyl}-2,2-dimethyl-5-oxo-hexahydro-imidazo[5,1-b]thiazole-3-carboxylic acid 2,2-dimethyl-propionyloxymethyl ester

Base Information

Chemical Name:(3S,7aR)-6-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetyl}-2,2-dimethyl-5-oxo-hexahydro-imidazo[5,1-b]thiazole-3-carboxylic acid 2,2-dimethyl-propionyloxymethyl ester
CAS No.:122692-95-9
Molecular Formula:C₃₉H₄₁N₅O₇S₂
Molecular Weight:755.916
Hs Code.:

(3S,7aR)-6-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetyl}-2,2-dimethyl-5-oxo-hexahydro-imidazo[5,1-b]thiazole-3-carboxylic acid 2,2-dimethyl-propionyloxymethyl ester

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Chemical Property of (3S,7aR)-6-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetyl}-2,2-dimethyl-5-oxo-hexahydro-imidazo[5,1-b]thiazole-3-carboxylic acid 2,2-dimethyl-propionyloxymethyl ester

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Technology Process of (3S,7aR)-6-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetyl}-2,2-dimethyl-5-oxo-hexahydro-imidazo[5,1-b]thiazole-3-carboxylic acid 2,2-dimethyl-propionyloxymethyl ester

There total 2 articles about (3S,7aR)-6-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetyl}-2,2-dimethyl-5-oxo-hexahydro-imidazo[5,1-b]thiazole-3-carboxylic acid 2,2-dimethyl-propionyloxymethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 66215-71-2
2-(2-tritylamino-thiazol-4-yl)-(Z)-2-methoxyiminoacetic acid

: 122692-95-9,122743-85-5
(3S,7aR)-6-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetyl}-2,2-dimethyl-5-oxo-hexahydro-imidazo[5,1-b]thiazole-3-carboxylic acid 2,2-dimethyl-propionyloxymethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: tetramethyl-α-chloroenamine / tetrahydrofuran / 3 h / 0 - 25 °C

2: 1.) lithium hexamethyldisilazide / 1.) THF, -70 deg C, 15 min; 2.) THF, -70 deg C -> r.t. and 20 deg C, 2 h

With tetramethyl-α-chloroenamine; lithium hexamethyldisilazane; In tetrahydrofuran;

Reference yield:

: 122692-71-1
pivaloyloxymethyl (2R,5R)-3,3-dimethyl-8-oxo-4-thia-7,1-diazabicyclo<3.3.0> octane-2-carboxylate

: 114586-19-5
2-(2-tritylamino-4-thiazolyl)-2-(methoxy-imino)acetyl chloride

: 122692-95-9,122743-85-5
(3S,7aR)-6-{2-[(Z)-Methoxyimino]-2-[2-(trityl-amino)-thiazol-4-yl]-acetyl}-2,2-dimethyl-5-oxo-hexahydro-imidazo[5,1-b]thiazole-3-carboxylic acid 2,2-dimethyl-propionyloxymethyl ester

Guidance literature:: With lithium hexamethyldisilazane; Yield given. Multistep reaction; 1.) THF, -70 deg C, 15 min; 2.) THF, -70 deg C -> r.t. and 20 deg C, 2 h;