methyl 3-<5-benzyloxy-2-methoxycarbonyl-3-(3-oxopentyl)phenoxy>-4,6-dimethoxy-2-pentylbenzoate

Base Information

Chemical Name:methyl 3-<5-benzyloxy-2-methoxycarbonyl-3-(3-oxopentyl)phenoxy>-4,6-dimethoxy-2-pentylbenzoate
CAS No.:122849-84-7
Molecular Formula:C₃₅H₄₂O₉
Molecular Weight:606.713
Hs Code.:

Synonyms:

Suppliers and Price of methyl 3-<5-benzyloxy-2-methoxycarbonyl-3-(3-oxopentyl)phenoxy>-4,6-dimethoxy-2-pentylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3-<5-benzyloxy-2-methoxycarbonyl-3-(3-oxopentyl)phenoxy>-4,6-dimethoxy-2-pentylbenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3-<5-benzyloxy-2-methoxycarbonyl-3-(3-oxopentyl)phenoxy>-4,6-dimethoxy-2-pentylbenzoate

There total 21 articles about methyl 3-<5-benzyloxy-2-methoxycarbonyl-3-(3-oxopentyl)phenoxy>-4,6-dimethoxy-2-pentylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 122849-82-5
methyl 3-<5-benzyloxy-2-methoxycarbonyl-3-(3-oxopentyl)phenoxy>-4-hydroxy-6-methoxy-2-pentylbenzoate

: 74-88-4
methyl iodide

: 122849-84-7
methyl 3-<5-benzyloxy-2-methoxycarbonyl-3-(3-oxopentyl)phenoxy>-4,6-dimethoxy-2-pentylbenzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 5h; Ambient temperature;

Reference yield:

: 24131-31-5
3,5-dibenzyloxybenzyl alcohol

: 122849-84-7
methyl 3-<5-benzyloxy-2-methoxycarbonyl-3-(3-oxopentyl)phenoxy>-4,6-dimethoxy-2-pentylbenzoate

Guidance literature:: Multi-step reaction with 15 steps

1: 95 percent / thionyl chloride, pyridine / CH₂Cl₂ / 3 h / Ambient temperature

2: 88 percent / dimethylformamide / 7 h / Ambient temperature

3: 91 percent / 30percent aq. sodium hydroxide / methanol / 72 h / Heating

4: 95 percent / potassium carbonate / acetone / 3 h / Heating

5: 95 percent / lithium aluminium hydride / diethyl ether / 2 h / Heating

6: 85 percent / pyridine / CHCl₃ / 3 h / 0 °C

7: 94 percent / 1,2-dimethoxyethane / dimethylsulfoxide / 18 h / Ambient temperature

8: 81 percent / ether / benzene / 1 h / Ambient temperature; aq. hydrochloric acid, ethyl acetate, 16 h

9: 98 percent / trifluoroacetic anhydride, / nitromethane / 1.5 h / 0 °C

10: 81 percent / H₂, conc. hydrochloric acid (4 drops) / 10percent palladized charcoal / ethyl acetate

11: 73 percent / potassium cyanoferrate(III), potassium carbonate / H₂O; dioxane / 0.17 h

12: 70 percent / various solvent(s) / 0.17 h / Heating

13: 94 percent / potassium carbonate / dimethylformamide / Ambient temperature

14: 66 percent / sodium methoxide / methanol / 3 h / Ambient temperature

15: 82 percent / potassium carbonate / dimethylformamide / 5 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; 1,2-dimethoxyethane; thionyl chloride; diethyl ether; hydrogen; sodium methylate; potassium carbonate; trifluoroacetic anhydride; potassium hexacyanoferrate(III); palladium on activated charcoal; In 1,4-dioxane; methanol; diethyl ether; nitromethane; dichloromethane; chloroform; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; benzene;

Reference yield:

: 58016-28-7
methyl 2,6-dihydroxy-6-pentylbenzoate

: 122849-84-7
methyl 3-<5-benzyloxy-2-methoxycarbonyl-3-(3-oxopentyl)phenoxy>-4,6-dimethoxy-2-pentylbenzoate

Guidance literature:: Multi-step reaction with 11 steps

1: 77 percent / potassium carbonate / acetone / 24 h / Heating

2: 89 percent / potassium carbonate / acetone / Heating

3: 80 percent / phosphoryl chloride / 24 h / 70 °C

4: 97 percent / sodium chlorite, sulphamic acid / H₂O; dioxane / 0.67 h

5: 98 percent / trifluoroacetic anhydride, / nitromethane / 1.5 h / 0 °C

6: 81 percent / H₂, conc. hydrochloric acid (4 drops) / 10percent palladized charcoal / ethyl acetate

7: 73 percent / potassium cyanoferrate(III), potassium carbonate / H₂O; dioxane / 0.17 h

8: 70 percent / various solvent(s) / 0.17 h / Heating

9: 94 percent / potassium carbonate / dimethylformamide / Ambient temperature

10: 66 percent / sodium methoxide / methanol / 3 h / Ambient temperature

11: 82 percent / potassium carbonate / dimethylformamide / 5 h / Ambient temperature

With hydrogenchloride; sodium chlorite; aminosulfonic acid; hydrogen; sodium methylate; potassium carbonate; trifluoroacetic anhydride; potassium hexacyanoferrate(III); trichlorophosphate; palladium on activated charcoal; In 1,4-dioxane; methanol; nitromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetone;