Methyl 4-{4-[(methanesulfonyl)oxy]butyl}benzoate

Base Information

Chemical Name:Methyl 4-{4-[(methanesulfonyl)oxy]butyl}benzoate
CAS No.:124656-56-0
Molecular Formula:C13H18O5S
Molecular Weight:286.349
Hs Code.:
DSSTox Substance ID:DTXSID70564164
Wikidata:Q82448763
Mol file:124656-56-0.mol

Synonyms:124656-56-0;Methyl 4-{4-[(methanesulfonyl)oxy]butyl}benzoate;SCHEMBL8732251;DTXSID70564164;F96695;METHYL 4-[4-(METHANESULFONYLOXY)BUTYL]BENZOATE

Suppliers and Price of Methyl 4-{4-[(methanesulfonyl)oxy]butyl}benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Methyl 4-{4-[(methanesulfonyl)oxy]butyl}benzoate

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:286.08749484
Heavy Atom Count:19
Complexity:363

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC(=O)C1=CC=C(C=C1)CCCCOS(=O)(=O)C

Technology Process of Methyl 4-{4-[(methanesulfonyl)oxy]butyl}benzoate

There total 3 articles about Methyl 4-{4-[(methanesulfonyl)oxy]butyl}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123910-88-3
methyl 4-(4-hydroxybut-1-yl)benzoate

: 124-63-0
methanesulfonyl chloride

: 124656-56-0
methyl 4-<(4-methylsulfonyloxy)butyl>benzoate

Guidance literature:: With triethylamine; In diethyl ether; at 0 - 20 ℃; for 4h; Yield given;

Reference yield:

: 619-42-1
4-methoxycarbonylphenyl bromide

: 124656-56-0
methyl 4-<(4-methylsulfonyloxy)butyl>benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 75.8 percent / triphenylphosphine, diethylamine, copper(I) iodide / palladium chloride / 18 h / Ambient temperature

2: 2.60 g / H₂ / 5percent palladium-on-charcoal / ethanol / 12 h / 2585.7 Torr

3: triethylamine / diethyl ether / 4 h / 0 - 20 °C

With copper(l) iodide; hydrogen; diethylamine; triethylamine; triphenylphosphine; palladium on activated charcoal; palladium dichloride; In diethyl ether; ethanol;

Reference yield:

: 123910-86-1
4-(4-hydroxybut-1-ynyl)benzoic acid methyl ester

: 124656-56-0
methyl 4-<(4-methylsulfonyloxy)butyl>benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 2.60 g / H₂ / 5percent palladium-on-charcoal / ethanol / 12 h / 2585.7 Torr

2: triethylamine / diethyl ether / 4 h / 0 - 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol;