Boc-Lys2(Cl)>-Pro ethyl ester

Base Information

Chemical Name:Boc-Lys2(Cl)>-Pro ethyl ester
CAS No.:111103-98-1
Molecular Formula:C₂₆H₃₈ClN₃O₇
Molecular Weight:540.057
Hs Code.:

Boc-Lys<Z<sup>2</sup>(Cl)>-Pro ethyl ester

Synonyms:

Suppliers and Price of Boc-Lys2(Cl)>-Pro ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boc-Lys2(Cl)>-Pro ethyl ester

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Technology Process of Boc-Lys2(Cl)>-Pro ethyl ester

There total 1 articles about Boc-Lys2(Cl)>-Pro ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33305-75-8,131477-20-8
L-proline ethyl ester monohydrochloride

: 62559-79-9
Boc-Lys2(Cl)>*t-butylamine

: 111103-98-1
Boc-Lys2(Cl)>-Pro ethyl ester

Guidance literature:: With 4-methyl-morpholine; sulfuric acid; dicyclohexyl-carbodiimide; Yield given. Multistep reaction; 1.) H₂O; 2.) 0 deg C, 20 min, chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight;

Reference yield:

: 111103-98-1
Boc-Lys2(Cl)>-Pro ethyl ester

: 111104-01-9
Boc-Ala-Lys2(Cl)>-Pro

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 6 M HCl / 1.) dioxane, RT, 1 h; 2.) ether, dioxane, RT, 2 h, overnight, refrigerator

2: 1.) N-methylmorpholine; 2.) DCCI / 2.) 0 deg C, 20 min, chloroform; 3.) chloroform, 0 deg C, 2 h, 5 deg C, overnight

3: 93 percent / 1 M NaOH / ethanol / 4 h / Ambient temperature

With 4-methyl-morpholine; hydrogenchloride; sodium hydroxide; dicyclohexyl-carbodiimide; In ethanol;

Reference yield:

: 111103-98-1
Boc-Lys2(Cl)>-Pro ethyl ester

: 111103-99-2
Lys2(Cl)>-Pro ethyl ester hydrochloride

Guidance literature:: With hydrogenchloride; Yield given. Multistep reaction; 1.) dioxane, RT, 1 h; 2.) ether, dioxane, RT, 2 h, overnight, refrigerator;