[(1S,2R,6R)-2-[2,6-Dimethoxy-4-(6-methoxy-benzofuran-2-yl)-phenyl]-6-(2,4-dimethoxy-phenyl)-4-methyl-cyclohex-3-enyl]-[2,4-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-methanone

Base Information

Chemical Name:[(1S,2R,6R)-2-[2,6-Dimethoxy-4-(6-methoxy-benzofuran-2-yl)-phenyl]-6-(2,4-dimethoxy-phenyl)-4-methyl-cyclohex-3-enyl]-[2,4-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-methanone
CAS No.:76502-88-0
Molecular Formula:C₄₆H₅₀O₉
Molecular Weight:746.898
Hs Code.:

[(1S,2R,6R)-2-[2,6-Dimethoxy-4-(6-methoxy-benzofuran-2-yl)-phenyl]-6-(2,4-dimethoxy-phenyl)-4-methyl-cyclohex-3-enyl]-[2,4-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-methanone

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Chemical Property of [(1S,2R,6R)-2-[2,6-Dimethoxy-4-(6-methoxy-benzofuran-2-yl)-phenyl]-6-(2,4-dimethoxy-phenyl)-4-methyl-cyclohex-3-enyl]-[2,4-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-methanone

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Technology Process of [(1S,2R,6R)-2-[2,6-Dimethoxy-4-(6-methoxy-benzofuran-2-yl)-phenyl]-6-(2,4-dimethoxy-phenyl)-4-methyl-cyclohex-3-enyl]-[2,4-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-methanone

There total 1 articles about [(1S,2R,6R)-2-[2,6-Dimethoxy-4-(6-methoxy-benzofuran-2-yl)-phenyl]-6-(2,4-dimethoxy-phenyl)-4-methyl-cyclohex-3-enyl]-[2,4-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 76472-89-4
chalcomoracin

: 77-78-1
dimethyl sulfate

: 76489-55-9
[(1S,2R,6R)-2-[2,6-Dimethoxy-4-(6-methoxy-benzofuran-2-yl)-phenyl]-6-(2,4-dimethoxy-phenyl)-4-methyl-cyclohex-3-enyl]-[2-hydroxy-4-methoxy-3-(3-methyl-but-2-enyl)-phenyl]-methanone

: 76502-88-0
[(1S,2R,6R)-2-[2,6-Dimethoxy-4-(6-methoxy-benzofuran-2-yl)-phenyl]-6-(2,4-dimethoxy-phenyl)-4-methyl-cyclohex-3-enyl]-[2,4-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-methanone

Guidance literature:: With potassium carbonate; In acetone; for 3h; Heating;
DOI:10.1246/cl.1980.1573

Reference yield: 61.0%

: 76502-88-0
[(1S,2R,6R)-2-[2,6-Dimethoxy-4-(6-methoxy-benzofuran-2-yl)-phenyl]-6-(2,4-dimethoxy-phenyl)-4-methyl-cyclohex-3-enyl]-[2,4-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-methanone

: 76489-56-0
trans-2,2',4,4'-tetramethoxy-3'-prenylchalcone

: 76489-57-1
2-[3,5-Dimethoxy-4-((E)-3-methyl-buta-1,3-dienyl)-phenyl]-6-methoxy-benzofuran

Guidance literature:: at 280 ℃; for 0.333333h; under 0.2 Torr;
DOI:10.1246/cl.1980.1573

Reference yield:

: 76502-88-0
[(1S,2R,6R)-2-[2,6-Dimethoxy-4-(6-methoxy-benzofuran-2-yl)-phenyl]-6-(2,4-dimethoxy-phenyl)-4-methyl-cyclohex-3-enyl]-[2,4-dimethoxy-3-(3-methyl-but-2-enyl)-phenyl]-methanone

: 76489-58-2
trimethyldihydromoracin C

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / 0.33 h / 280 °C / 0.2 Torr

2: H₂ / Pd-CaCO₃

With hydrogen; Lindlar's catalyst;
DOI:10.1246/cl.1980.1573