cis-4-hydroxy-3-methyl-6-phenylhexanoic lactone

Base Information

Chemical Name:cis-4-hydroxy-3-methyl-6-phenylhexanoic lactone
CAS No.:102519-59-5
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

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Chemical Property of cis-4-hydroxy-3-methyl-6-phenylhexanoic lactone

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Technology Process of cis-4-hydroxy-3-methyl-6-phenylhexanoic lactone

There total 15 articles about cis-4-hydroxy-3-methyl-6-phenylhexanoic lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: rac-(4R,5S)-4-methyl-5-phenethyltetrahydro-2-furanol

: 102519-59-5,102519-60-8,128756-47-8,144939-68-4,144939-69-5
trans-4-hydroxy-3-methyl-6-phenylhexanoic lactone

Guidance literature:: With N-chloro-succinimide; 4-ethanoyloxy-2,2,6,6-tetramethyl-piperidinyloxy; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate; In dichloromethane; water; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1002/chem.201100049

Reference yield: 91.0%

: 1206535-29-6
2-bromoacetic acid 1-phenethylallyl ester

: 102519-59-5,102519-60-8,128756-47-8,144939-68-4,144939-69-5
trans-4-hydroxy-3-methyl-6-phenylhexanoic lactone

Guidance literature:: 2-bromoacetic acid 1-phenethylallyl ester; With diisobutylaluminium hydride; In toluene; at -78 ℃; Inert atmosphere;

With triethyl borane; tri-n-butyl-tin hydride; In toluene; at -70 ℃; Inert atmosphere;

With benzaldehyde; In toluene; at -70 - 25 ℃; for 4h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/asia.201200212

Reference yield: 46.0%

: 1206535-29-6
2-bromoacetic acid 1-phenethylallyl ester

: 102519-59-5,102519-60-8,128756-47-8,144939-68-4,144939-69-5
trans-4-hydroxy-3-methyl-6-phenylhexanoic lactone

: 103240-88-6
5-phenylpenten-3-yl acetate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 6h; Reflux; Inert atmosphere;
DOI:10.1002/asia.201200212