Technology Process of C35H53N9O11
There total 4 articles about C35H53N9O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-hydroxyethyl acetate; BocNH-C(=NBoc)-SCH2-terminated resin;
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 20 ℃;
(3'S,5RS)-5-[N-(6-amino-3-benzyloxycarbonylaminohexanoyl)-N-methylamino]-5,6-dihydro-2-ureidopyrimid-4(1H)-one hydrochloride;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 72h;
DOI:10.3390/70600469
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 60 percent / EDC
2.1: 100 percent / HCl / dioxane
3.1: Ph3P; DIAD / tetrahydrofuran / 20 °C
3.2: DBU / dimethylformamide / 72 h / 20 °C
With
hydrogenchloride; di-isopropyl azodicarboxylate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane;
3.1: Mitsunobu reaction;
DOI:10.3390/70600469
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 60 percent / EDC
2.1: 100 percent / HCl / dioxane
3.1: Ph3P; DIAD / tetrahydrofuran / 20 °C
3.2: DBU / dimethylformamide / 72 h / 20 °C
With
hydrogenchloride; di-isopropyl azodicarboxylate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane;
3.1: Mitsunobu reaction;
DOI:10.3390/70600469
