[Mo(CO)3CH₃C(CH₂P(C₂H₅)(C₆H₅))3]

Base Information

Chemical Name:[Mo(CO)3CH₃C(CH₂P(C₂H₅)(C₆H₅))3]
CAS No.:153956-41-3
Molecular Formula:C₃₂H₃₉MoO₃P₃
Molecular Weight:660.521
Hs Code.:

[Mo(CO)3CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>2</sub>H<sub>5</sub>)(C<sub>6</sub>H<sub>5</sub>))3]

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Mo(CO)3CH₃C(CH₂P(C₂H₅)(C₆H₅))3]

Chemical Property:

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Technology Process of [Mo(CO)3CH₃C(CH₂P(C₂H₅)(C₆H₅))3]

There total 2 articles about [Mo(CO)3CH₃C(CH₂P(C₂H₅)(C₆H₅))3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 74-96-4
ethyl bromide

: 15038-48-9,17731-95-2
tris(acetonitrile)tricarbonylmolybdenum⁽⁰⁾

: 153888-54-1,154002-80-9,190376-24-0
H₃CC(CH₂P(C₆H₅)H)3

: 153956-41-3,154006-92-5
[Mo(CO)3CH₃C(CH₂P(C₂H₅)(C₆H₅))3]

Guidance literature:: With MeLi; In tetrahydrofuran; diethyl ether; (argon); addn. of MeLi in Et2O at 0°C with stirring to the ligandin THF, warming to room temp., stirring (2 h), addn. of the Mo complex, stirring (20 h), cooling to 0°C, addn. of the halide, warming to room temp., stirring (48 h); evapn., dissoln. (CH2Cl2), filtration through silica gel and Kieselgur, elution with CH2Cl2, evapn., drying (vac., 1 d);
DOI:10.1002/cber.19971301006

Reference yield:

: 15038-48-9,17731-95-2
tris(acetonitrile)tricarbonylmolybdenum⁽⁰⁾

: 154002-81-0
H₃CC(CH₂P(C₆H₅)C₂H₅)3

: 153956-41-3,154006-92-5
[Mo(CO)3CH₃C(CH₂P(C₂H₅)(C₆H₅))3]

Guidance literature:: In dichloromethane; (N2); stirred overnight at 20°C; filtered through silica gel, added petroleum ether, filtered through silica gel, solvent removed (vac.), recrystd. (CH2Cl2/ petroleum ether), dried (vac.); elem. anal.;
DOI:10.1016/0022-328X(93)80458-N