trans bis[1-methyl-3-(p-nitrophenyl)triazenido 1-oxide-κ(2)N(3),O]dipyridinenickel(II)

Base Information

Chemical Name:trans bis[1-methyl-3-(p-nitrophenyl)triazenido 1-oxide-κ(2)N(3),O]dipyridinenickel(II)
CAS No.:500715-89-9
Molecular Formula:C₂₄H₂₄N₁₀NiO₆
Molecular Weight:607.208
Hs Code.:

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Chemical Property of trans bis[1-methyl-3-(p-nitrophenyl)triazenido 1-oxide-κ(2)N(3),O]dipyridinenickel(II)

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Technology Process of trans bis[1-methyl-3-(p-nitrophenyl)triazenido 1-oxide-κ(2)N(3),O]dipyridinenickel(II)

There total 1 articles about trans bis[1-methyl-3-(p-nitrophenyl)triazenido 1-oxide-κ(2)N(3),O]dipyridinenickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 110-86-1
pyridine

: bis(triphenylphosphine)-nickel(II)chloride

: 86796-97-6
1-methyl-3-(p-nitrophenyl)triazene 1-oxide

: 500715-89-9
trans bis[1-methyl-3-(p-nitrophenyl)triazenido 1-oxide-κ(2)N(3),O]dipyridinenickel(II)

Guidance literature:: With (CH₃CH₂)3N; In methanol; ethyl acetate; to warm soln. of NiCl2(PPh3)3 (1 mol) in MeOH/EtOAc (2:1) soln. 1-methyl-3-(p-nitrophenyl)triazene 1-oxide (2 mol) in MeOH and Et3N added under stirring and heating; after 10 min pyridine added; stirring 1 h; slow evapn. at room temp.;
DOI:10.1107/S0108270102019820