[Os₃(C₆H₅N)2(CO)9]

Base Information

Chemical Name:[Os₃(C₆H₅N)2(CO)9]
CAS No.:102869-60-3
Molecular Formula:C₂₁H₁₀N₂O₉Os₃
Molecular Weight:1004.92
Hs Code.:

[Os<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>N)2(CO)9]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Os₃(C₆H₅N)2(CO)9]

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Technology Process of [Os₃(C₆H₅N)2(CO)9]

There total 2 articles about [Os₃(C₆H₅N)2(CO)9] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 15696-40-9
dodecacarbonyl triosmium

: 586-96-9
Nitrosobenzene

: 102869-60-3
[Os₃(C₆H₅N)2(CO)9]

Guidance literature:: With carbon monoxide; In octane; High Pressure; flushing of a soln. of the Os compd. and nitrosobenzene in octane with CO and heating in an evacuated tube with CO (15 psig) to 126°C for 24 h; cooling to room temp., depressurizing, filtn., column chromy. of the filtrate on silica gel and elution with hexane;

Reference yield: 19.0%

: 15696-40-9
dodecacarbonyl triosmium

: 586-96-9
Nitrosobenzene

: 102869-57-8
Os3(μ3-NPh)(CO)10

: 102869-60-3
[Os₃(C₆H₅N)2(CO)9]

Guidance literature:: In octane; refluxed under N2 for 7 h; cooling to room temp., filtn., column chromy. of the filtrate on silicagel and elution with CH2Cl2-hexane; elem. anal.;