C₃₁H₅₂O₆Si

Base Information

Chemical Name:C₃₁H₅₂O₆Si
CAS No.:1300655-94-0
Molecular Formula:C₃₁H₅₂O₆Si
Molecular Weight:548.836
Hs Code.:

C<sub>31</sub>H<sub>52</sub>O<sub>6</sub>Si

Synonyms:

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Chemical Property of C₃₁H₅₂O₆Si

Chemical Property:

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Technology Process of C₃₁H₅₂O₆Si

There total 12 articles about C₃₁H₅₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300655-86-0
C₁₃H₁₈O₂

: 1300655-94-0
C₃₁H₅₂O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: n-butyllithium / hexane; tert-butyl methyl ether / 0.17 h / -78 °C / Inert atmosphere

1.2: 0.67 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / hexane / 2 h / Inert atmosphere; Reflux

3.1: acetylacetonatodicarbonylrhodium(l) / benzene / 4.5 h / 60 °C / 51716.2 Torr / Autoclave

3.2: 1 h / 40 °C / Inert atmosphere

4.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

5.2: -78 - 20 °C / Inert atmosphere

6.1: toluene / 18 h / Inert atmosphere; Reflux

7.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; citric acid / tetrahydrofuran; tert-butyl alcohol / 24 h / Inert atmosphere

8.1: sodium periodate; sodium hydrogencarbonate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

9.1: tetra-(n-butyl)ammonium iodide / dichloromethane; water / 3 h / Inert atmosphere

With 2,6-dimethylpyridine; acetylacetonatodicarbonylrhodium(l); sodium periodate; osmium(VIII) oxide; n-butyllithium; water; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; citric acid; In tetrahydrofuran; hexane; dichloromethane; tert-butyl methyl ether; water; toluene; tert-butyl alcohol; benzene; 9.1: Felkin addition;
DOI:10.1021/ja201467z

Reference yield:

: 1300655-89-3
C₂₁H₃₂O₄

: 1300655-94-0
C₃₁H₅₂O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

3.1: toluene / 18 h / Inert atmosphere; Reflux

4.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; citric acid / tetrahydrofuran; tert-butyl alcohol / 24 h / Inert atmosphere

5.1: sodium periodate; sodium hydrogencarbonate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

6.1: tetra-(n-butyl)ammonium iodide / dichloromethane; water / 3 h / Inert atmosphere

With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; water; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; citric acid; In tetrahydrofuran; hexane; dichloromethane; water; toluene; tert-butyl alcohol; 6.1: Felkin addition;
DOI:10.1021/ja201467z

Reference yield:

: 1300655-90-6
C₂₇H₄₆O₄Si

: 1300655-94-0
C₃₁H₅₂O₆Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: toluene / 18 h / Inert atmosphere; Reflux

3.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; citric acid / tetrahydrofuran; tert-butyl alcohol / 24 h / Inert atmosphere

4.1: sodium periodate; sodium hydrogencarbonate / tetrahydrofuran; water / 1 h / 0 °C / Inert atmosphere

5.1: tetra-(n-butyl)ammonium iodide / dichloromethane; water / 3 h / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; water; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; citric acid; In tetrahydrofuran; hexane; dichloromethane; water; toluene; tert-butyl alcohol; 5.1: Felkin addition;
DOI:10.1021/ja201467z