[Fe3(μ3-O)(O2CPh)5(salicylaldehyde oxime(2-))2(EtOH)(H2O)]

Base Information

• Chemical Name: [Fe3(μ3-O)(O2CPh)5(salicylaldehyde oxime(2-))2(EtOH)(H2O)]
• CAS No.: 881212-93-7
• Molecular Formula: C₄₄H₃₈Fe₃NO₁₅
• Molecular Weight: 988.324
• Mol file: 881212-93-7.mol

Synonyms:

Chemical Property of [Fe3(μ3-O)(O2CPh)5(salicylaldehyde oxime(2-))2(EtOH)(H2O)]

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [Fe3(μ3-O)(O2CPh)5(salicylaldehyde oxime(2-))2(EtOH)(H2O)]

There total 1 articles about [Fe3(μ3-O)(O2CPh)5(salicylaldehyde oxime(2-))2(EtOH)(H2O)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

ethanol (64-17-5) + salicylaldehyde-oxime (94-67-7) + [Fe3(μ3-O)(O2CPh)6(H2O)2(OH)] → [Fe3(μ3-O)(O2CPh)5(salicylaldehyde oxime(2-))2(EtOH)(H2O)] (881212-93-7)

Guidance literature:

In ethanol; H2salox was added to refluxing soln. Fe complex in EtOH and refluxed for1 h; soln. was filtered and kept for 2 weeks, ppt. was filtered, washed with cold MeOH and dried in vacuo;

DOI:10.1021/ic051945q

Reference yield:

[Fe3(μ3-O)(O2CPh)5(salicylaldehyde oxime(2-))2(EtOH)(H2O)] (881212-93-7) + acetonitrile (75-05-8,26809-02-9) → [Fe6(μ3-O)2(O2CPh)10(salicylaldoxime(2-))2(H2O)2]*2MeCN*3H2O

Guidance literature:

In acetonitrile; soln. Fe complex in MeCN was refluxed for 5 h; ppt. was filtered, washed with cold MeCN and dried in vacuo;

DOI:10.1021/ic051945q

upstream raw materials:

ethanol

salicylaldehyde-oxime