Sodium; (2S,5R,6R)-3,3-dimethyl-7-oxo-6-{3-[(E)-2-(3,4,5-trimethoxy-phenyl)-vinyl]-ureido}-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

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Chemical Name:Sodium; (2S,5R,6R)-3,3-dimethyl-7-oxo-6-{3-[(E)-2-(3,4,5-trimethoxy-phenyl)-vinyl]-ureido}-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate
CAS No.:78974-19-3
Molecular Formula:C₂₀H₂₄N₃O₇S*Na
Molecular Weight:473.482
Hs Code.:

Synonyms:

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Chemical Property of Sodium; (2S,5R,6R)-3,3-dimethyl-7-oxo-6-{3-[(E)-2-(3,4,5-trimethoxy-phenyl)-vinyl]-ureido}-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

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Technology Process of Sodium; (2S,5R,6R)-3,3-dimethyl-7-oxo-6-{3-[(E)-2-(3,4,5-trimethoxy-phenyl)-vinyl]-ureido}-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

There total 4 articles about Sodium; (2S,5R,6R)-3,3-dimethyl-7-oxo-6-{3-[(E)-2-(3,4,5-trimethoxy-phenyl)-vinyl]-ureido}-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 551-16-6
6-Aminopenicillanic Acid

: 78974-19-3
Sodium; (2S,5R,6R)-3,3-dimethyl-7-oxo-6-{3-[(E)-2-(3,4,5-trimethoxy-phenyl)-vinyl]-ureido}-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 3 h

2: 2.) sodium 2-ethylhexanoate / 1.) toluene, acetonitrile, RT, 18 h, 2.) ether, THF

With sodium 2-ethylhexanoic acid; In acetonitrile;
DOI:10.1021/jm00142a024

Reference yield:

: (E)-3-(3,4,5-Trimethoxy-phenyl)-acryloyl azide

: 78974-19-3
Sodium; (2S,5R,6R)-3,3-dimethyl-7-oxo-6-{3-[(E)-2-(3,4,5-trimethoxy-phenyl)-vinyl]-ureido}-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 1 h / Heating

2: 2.) sodium 2-ethylhexanoate / 1.) toluene, acetonitrile, RT, 18 h, 2.) ether, THF

With sodium 2-ethylhexanoic acid; In toluene;
DOI:10.1021/jm00142a024

Reference yield:

: 10263-19-1,89652-61-9
(E)-3-(3,4,5-trimethoxyphenyl)acryloyl chloride

: 78974-19-3
Sodium; (2S,5R,6R)-3,3-dimethyl-7-oxo-6-{3-[(E)-2-(3,4,5-trimethoxy-phenyl)-vinyl]-ureido}-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / H₂O / 1 h / 0 °C

2: toluene / 1 h / Heating

3: 2.) sodium 2-ethylhexanoate / 1.) toluene, acetonitrile, RT, 18 h, 2.) ether, THF

With sodium azide; sodium 2-ethylhexanoic acid; In water; toluene;
DOI:10.1021/jm00142a024