3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

Base Information

Chemical Name:3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al
CAS No.:101471-66-3
Molecular Formula:C₁₉H₂₀O₄S
Molecular Weight:344.431
Hs Code.:

3-<methoxy(phenylthio)methyl>-2-(3,4-dimethoxyphenyl)prop-2-en-1-al

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

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Technology Process of 3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

There total 1 articles about 3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13865-50-4
methoxymethyl phenyl sulfide

: 85907-71-7
3-(dimethylamino)-2-(3,4-dimethoxyphenyl)prop-2-en-1-al

: 99706-75-9,101471-66-3
3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; Yield given. Multistep reaction; 1.) THF,cyclohexane, -78 deg C, 2.5 h, 2.) THF, cyclohexane, -78 deg C, 27 h;
DOI:10.1021/jo00359a057

Reference yield:

: 99706-75-9,101471-66-3
3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

: 21104-34-7
N-methyl-3a-<3,4-(dimethoxy)phenyl>-2,3,3a,4,5,6,7,7a-octahydroindole-2,6-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 1,5-diazabicyclo<4.3.0>non-5-ene, 2.) EtONa / 1.) THF, RT,10 h, 2.) THF, EtOH, reflux, 24 h

2: p-toluenesulfonic acid / tetrahydrofuran; H₂O / 6 h / Heating

3: 71 percent / tetrahydrofuran / 10 h / 80 °C

With DBN; sodium ethanolate; toluene-4-sulfonic acid; In tetrahydrofuran; water;
DOI:10.1021/jo00359a057

Reference yield:

: 99706-75-9,101471-66-3
3--2-(3,4-dimethoxyphenyl)prop-2-en-1-al

: 101471-67-4
4-(carbomethoxymethyl)-4-(3,4-dimethoxyphenyl)cyclohex-2-en-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1,5-diazabicyclo<4.3.0>non-5-ene, 2.) EtONa / 1.) THF, RT,10 h, 2.) THF, EtOH, reflux, 24 h

2: p-toluenesulfonic acid / tetrahydrofuran; H₂O / 6 h / Heating

With DBN; sodium ethanolate; toluene-4-sulfonic acid; In tetrahydrofuran; water;
DOI:10.1021/jo00359a057