(3,5-dimethyl-4-isothiazolyl)methyl-p-tolyl sulphone

Base Information

Chemical Name:(3,5-dimethyl-4-isothiazolyl)methyl-p-tolyl sulphone
CAS No.:118157-19-0
Molecular Formula:C₁₃H₁₅NO₂S₂
Molecular Weight:281.4
Hs Code.:

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Chemical Property of (3,5-dimethyl-4-isothiazolyl)methyl-p-tolyl sulphone

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Technology Process of (3,5-dimethyl-4-isothiazolyl)methyl-p-tolyl sulphone

There total 4 articles about (3,5-dimethyl-4-isothiazolyl)methyl-p-tolyl sulphone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53064-43-0
4-hydroxymethyl-3,5-dimethylisothiazole

: 118157-19-0
(3,5-dimethyl-4-isothiazolyl)methyl-p-tolyl sulphone

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / SOCl₂ / benzene / 3 h / Ambient temperature

2: 79 percent / dimethylformamide / 24 h / Ambient temperature

With thionyl chloride; In N,N-dimethyl-formamide; benzene;

Reference yield:

: 91367-85-0
3,5-dimethyl-4-isothiazolylcarboxyaldehyde

: 118157-19-0
(3,5-dimethyl-4-isothiazolyl)methyl-p-tolyl sulphone

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / NaBH₄, 0.2N NaOH / H₂O; methanol / 3 h / Ambient temperature

2: 75 percent / SOCl₂ / benzene / 3 h / Ambient temperature

3: 79 percent / dimethylformamide / 24 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; thionyl chloride; In methanol; water; N,N-dimethyl-formamide; benzene;

Reference yield:

: 113234-27-8
3,5-dimethyl-4-iodoisothiazole

: 118157-19-0
(3,5-dimethyl-4-isothiazolyl)methyl-p-tolyl sulphone

Guidance literature:: Multi-step reaction with 5 steps

1: 76 percent / 0.5 h / 200 °C

2: 75 percent / diisobutylaluminium hydride / toluene / 1.) -78 deg C, 8 h; 2.) 0 deg C

3: 82 percent / NaBH₄, 0.2N NaOH / H₂O; methanol / 3 h / Ambient temperature

4: 75 percent / SOCl₂ / benzene / 3 h / Ambient temperature

5: 79 percent / dimethylformamide / 24 h / Ambient temperature

With sodium hydroxide; sodium tetrahydroborate; thionyl chloride; diisobutylaluminium hydride; In methanol; water; N,N-dimethyl-formamide; toluene; benzene;