bis<2,6-bis(trifluoromethyl)phenyl>diphosphene

Base Information

Chemical Name:bis<2,6-bis(trifluoromethyl)phenyl>diphosphene
CAS No.:115044-05-8
Molecular Formula:C₁₆H₆F₁₂P₂
Molecular Weight:488.152
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis<2,6-bis(trifluoromethyl)phenyl>diphosphene

Chemical Property:

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Technology Process of bis<2,6-bis(trifluoromethyl)phenyl>diphosphene

There total 5 articles about bis<2,6-bis(trifluoromethyl)phenyl>diphosphene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 402-31-3
1,3-bis(trifluoromethyl)benzene

: 115044-05-8
bis<2,6-bis(trifluoromethyl)phenyl>diphosphene

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / phosphorus trichloride, n-buthyllithium*TMEDA / diethyl ether / -78 - 20 °C

2: 80 percent / tributyltinhydride / diethyl ether / 2 h / Ambient temperature

3: 1.) germaniumtetrachloride; 2.) DBU / 1.) dioxane, 110 deg C, 24 h; 2.) benzene

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; tri-n-butyl-tin hydride; germaniumtetrachloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; phosphorus trichloride; In diethyl ether;

Reference yield:

: 115044-02-5
<2,6-bis(trifluoromethyl)phenyl>dichlorophosphine

: 115044-05-8
bis<2,6-bis(trifluoromethyl)phenyl>diphosphene

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / tributyltinhydride / diethyl ether / 2 h / Ambient temperature

2: 1.) germaniumtetrachloride; 2.) DBU / 1.) dioxane, 110 deg C, 24 h; 2.) benzene

With tri-n-butyl-tin hydride; germaniumtetrachloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In diethyl ether;

Reference yield:

: 115044-03-6
[2,6-bis(trifluoromethyl)phenyl]phosphane

: 115044-05-8
bis<2,6-bis(trifluoromethyl)phenyl>diphosphene

Guidance literature:: With germaniumtetrachloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; Yield given. Multistep reaction; 1.) dioxane, 110 deg C, 24 h; 2.) benzene;