3,5-dideuterio-4-iodotoluene

Base Information

• Chemical Name: 3,5-dideuterio-4-iodotoluene
• CAS No.: 740872-00-8
• Molecular Formula: C₇H₇I
• Molecular Weight: 220.021

Synonyms:

Chemical Property of 3,5-dideuterio-4-iodotoluene

Chemical Property:

Purity/Quality:

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Technology Process of 3,5-dideuterio-4-iodotoluene

There total 2 articles about 3,5-dideuterio-4-iodotoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-toluidine hydrochloride (540-23-8) → 3,5-dideuterio-4-iodotoluene (740872-00-8)

Guidance literature:

p-toluidine hydrochloride; With hydrogenchloride; sodium nitrite;

With potassium iodide;

DOI:10.1021/jo040123s

Reference yield:

2,6-dideuterio p-toludine hydrochloride → 3,5-dideuterio-4-iodotoluene (740872-00-8)

Guidance literature:

With diazotization reagent; potassium iodide;

DOI:10.1021/jo0205715

Reference yield:

sodium 2,2,2-trifluoroacetate (2923-18-4) + 3,5-dideuterio-4-iodotoluene (740872-00-8) → 2,6-dideuterio-4-methylbenzotrifluoride

Guidance literature:

With copper(l) iodide; In 1-methyl-pyrrolidin-2-one; at 160 ℃;

DOI:10.1021/jo0205715

upstream raw materials:

p-toluidine hydrochloride

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