4-[trans-4-(4'-cyano-4-biphenylyl)cyclohexyl]butyraldehyde

Base Information

Chemical Name:4-[trans-4-(4'-cyano-4-biphenylyl)cyclohexyl]butyraldehyde
CAS No.:101160-83-2
Molecular Formula:C₂₃H₂₅NO
Molecular Weight:331.458
Hs Code.:

Synonyms:

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Chemical Property of 4-[trans-4-(4'-cyano-4-biphenylyl)cyclohexyl]butyraldehyde

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Technology Process of 4-[trans-4-(4'-cyano-4-biphenylyl)cyclohexyl]butyraldehyde

There total 11 articles about 4-[trans-4-(4'-cyano-4-biphenylyl)cyclohexyl]butyraldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78531-65-4
4-([1,1'-biphenyl]-4-yl)cyclohexan-1-one

: 101160-83-2
4-[trans-4-(4'-cyano-4-biphenylyl)cyclohexyl]butyraldehyde

Guidance literature:: Multi-step reaction with 10 steps

1: aluminium chloride / 1,2-dichloro-ethane / 0.17 h / Ambient temperature

2: 15percent aq. NH₄OH / 12 h / 15 °C

3: 76 percent / benzenesulfonyl chloride / pyridine / 1 h / 72 °C

4: 81 percent / tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

5: 61 percent / 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

6: tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

7: 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

8: tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

9: 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

10: 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

With hydrogenchloride; ammonium hydroxide; aluminium trichloride; benzenesulfonyl chloride; In tetrahydrofuran; pyridine; 1,2-dichloro-ethane;

Reference yield:

: 101160-76-3
4-(4'-cyano-4-biphenylyl)cyclohexanone

: 101160-83-2
4-[trans-4-(4'-cyano-4-biphenylyl)cyclohexyl]butyraldehyde

Guidance literature:: Multi-step reaction with 7 steps

1: 81 percent / tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

2: 61 percent / 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

3: tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

4: 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

5: tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

6: 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

7: 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

With hydrogenchloride; In tetrahydrofuran;

Reference yield:

: 101241-33-2
4'-(4-oxocyclohexyl)-4-biphenylcarboxamide

: 101160-83-2
4-[trans-4-(4'-cyano-4-biphenylyl)cyclohexyl]butyraldehyde

Guidance literature:: Multi-step reaction with 8 steps

1: 76 percent / benzenesulfonyl chloride / pyridine / 1 h / 72 °C

2: 81 percent / tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

3: 61 percent / 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

4: tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

5: 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

6: tetrahydrofuran; various solvent(s) / 2.75 h / Ambient temperature

7: 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

8: 2N aq. HCl / tetrahydrofuran / 0.5 h / Heating

With hydrogenchloride; benzenesulfonyl chloride; In tetrahydrofuran; pyridine;