(+/-)-bibenzyl/p-cannabicyclol hybrid

Base Information

• Chemical Name: (+/-)-bibenzyl/p-cannabicyclol hybrid
• CAS No.: 120467-16-5
• Molecular Formula: C₂₄H₂₈O₂
• Molecular Weight: 348.485
• Mol file: 120467-16-5.mol

Synonyms:

Chemical Property of (+/-)-bibenzyl/p-cannabicyclol hybrid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-bibenzyl/p-cannabicyclol hybrid

There total 4 articles about (+/-)-bibenzyl/p-cannabicyclol hybrid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

(+/-)-bibenzyl/p-cannabichromene hybrid (120467-13-2) → (+/-)-bibenzyl/p-cannabicyclol hybrid (120467-16-5)

Guidance literature:

In acetone; Irradiation;

DOI:10.1039/P19880001263

Reference yield:

1,3-dimethoxy-5-(2-phenylethyl)benzene (78916-50-4) → (+/-)-bibenzyl/p-cannabicyclol hybrid (120467-16-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 71 percent / BBr₃ / CH₂Cl₂ / 1.) -70 deg C, 2.) room temp., 2 h

2: 15 percent / 2,6-di-t-butyl pyridine / 5.5 h / 160 °C

3: 18 percent / acetone / Irradiation

With 2,6-di-tert-butyl-pyridine; boron tribromide; In dichloromethane; acetone;

DOI:10.1039/P19880001263

Reference yield:

(E/Z)-3,7-dimethyl-2,6-octadienal (5392-40-5,96680-15-8) → (+/-)-bibenzyl/p-cannabicyclol hybrid (120467-16-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 15 percent / 2,6-di-t-butyl pyridine / 5.5 h / 160 °C

2: 18 percent / acetone / Irradiation

With 2,6-di-tert-butyl-pyridine; In acetone;

DOI:10.1039/P19880001263

upstream raw materials:

dihydropinosylvin

(E/Z)-3,7-dimethyl-2,6-octadienal

(+/-)-bibenzyl/p-cannabichromene hybrid

1,3-dimethoxy-5-(2-phenylethyl)benzene