2,6-di-p-toluyl-1,3,5,7-tetraoxa-2,6-dibora-4,8-octalindione

Base Information

Chemical Name:2,6-di-p-toluyl-1,3,5,7-tetraoxa-2,6-dibora-4,8-octalindione
CAS No.:87841-20-1
Molecular Formula:C₁₈H₁₄B₂O₆
Molecular Weight:347.928
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,6-di-p-toluyl-1,3,5,7-tetraoxa-2,6-dibora-4,8-octalindione

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Technology Process of 2,6-di-p-toluyl-1,3,5,7-tetraoxa-2,6-dibora-4,8-octalindione

There total 1 articles about 2,6-di-p-toluyl-1,3,5,7-tetraoxa-2,6-dibora-4,8-octalindione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 87720-44-3
BO₂C₃(C₂H₅)(O)C(O)OB(C₂H₅)O

: 5084-80-0
tri(4-tolyl)boroxine

: 87841-20-1
2,6-di-p-toluyl-1,3,5,7-tetraoxa-2,6-dibora-4,8-octalindione

Guidance literature:: In benzene; a mixt. of octahydroxycyclobutane and tris(4-methylphenylboroxine) in benzene were refluxed for 2 h; during the reaction the starting materialsdissolved and the product pptd. as a crystn. solid; after cooling it was filtered and washed with benzene and pentane, sublimation at 150°C at high vac. gave a colorless solid, further purifn. by high vac. sublimation at ca 130-150°C or by crystn. from a large vol. of toluene; elem. anal.;