Technology Process of C21H23NO3
There total 9 articles about C21H23NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: magnesium / diethyl ether
2.1: diethyl ether
3.1: acetic acid / 3 h / Reflux
4.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 12 h / Reflux
5.1: sodium hydride / tetrahydrofuran / Inert atmosphere
5.2: Inert atmosphere; Reflux
6.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere
7.1: ethylenediamine / methanol / 0.5 h / 20 °C
8.1: tetrahydrofuran
With
N-Bromosuccinimide; sodium hydride; magnesium; acetic acid; ethylenediamine; triphenylphosphine; diethylazodicarboxylate; dibenzoyl peroxide;
In
tetrahydrofuran; methanol; tetrachloromethane; diethyl ether;
DOI:10.1055/s-0030-1259977
- Guidance literature:
-
Multi-step reaction with 2 steps
1: ethylenediamine / methanol / 0.5 h / 20 °C
2: tetrahydrofuran
With
ethylenediamine;
In
tetrahydrofuran; methanol;
DOI:10.1055/s-0030-1259977
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 12 h / Reflux
2.1: sodium hydride / tetrahydrofuran / Inert atmosphere
2.2: Inert atmosphere; Reflux
3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 12 h / 0 °C / Inert atmosphere
4.1: ethylenediamine / methanol / 0.5 h / 20 °C
5.1: tetrahydrofuran
With
N-Bromosuccinimide; sodium hydride; ethylenediamine; triphenylphosphine; diethylazodicarboxylate; dibenzoyl peroxide;
In
tetrahydrofuran; methanol; tetrachloromethane;
DOI:10.1055/s-0030-1259977
