Technology Process of C39H46N6O9
There total 10 articles about C39H46N6O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: DCC / dioxane; CH2Cl2
2: 0.2 N aq. NaOH / methanol; acetonitrile
3: H2 / 5percent Pd/C
4: 39 percent / DCC / dioxane
5: 100 percent / AlCl3, EtSH
With
sodium hydroxide; aluminium trichloride; hydrogen; dicyclohexyl-carbodiimide; ethanethiol;
palladium on activated charcoal;
In
1,4-dioxane; methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00389a068
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 76 percent / DCC / dioxane
2: 5.2 percent / Tl(NO3)2 (TTN) / Ambient temperature
3: Zn, 90percent aq. AcOH / Ambient temperature
4: diethyl ether; methanol
5: H2, AcOK / 5percent Pd/C / methanol
6: DCC / dioxane; CH2Cl2
7: 0.2 N aq. NaOH / methanol; acetonitrile
8: H2 / 5percent Pd/C
9: 39 percent / DCC / dioxane
10: 100 percent / AlCl3, EtSH
With
sodium hydroxide; aluminium trichloride; Tl(NO3)2; hydrogen; potassium acetate; acetic acid; dicyclohexyl-carbodiimide; ethanethiol; zinc;
palladium on activated charcoal;
In
1,4-dioxane; methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo00389a068
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 76 percent / DCC / dioxane
2: 5.2 percent / Tl(NO3)2 (TTN) / Ambient temperature
3: Zn, 90percent aq. AcOH / Ambient temperature
4: diethyl ether; methanol
5: H2, AcOK / 5percent Pd/C / methanol
6: DCC / dioxane; CH2Cl2
7: 0.2 N aq. NaOH / methanol; acetonitrile
8: H2 / 5percent Pd/C
9: 39 percent / DCC / dioxane
10: 100 percent / AlCl3, EtSH
With
sodium hydroxide; aluminium trichloride; Tl(NO3)2; hydrogen; potassium acetate; acetic acid; dicyclohexyl-carbodiimide; ethanethiol; zinc;
palladium on activated charcoal;
In
1,4-dioxane; methanol; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo00389a068